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ENERGY <br />y ABORATORIES <br />Client: Cotter Corporation <br />Project: Schwartz SW 7/13/11 S25884- S25886 <br />Analyte Count Result Units <br />Method: E200.8 <br />Sample ID: C11070550- 005CMSD <br />Potassium <br />Silver <br />Sodium <br />Thallium <br />Uranium <br />Zinc <br />Sample ID: LRB <br />Antimony <br />Calcium <br />Copper <br />Iron <br />Magnesium <br />Manganese <br />Molybdenum <br />Potassium <br />Silver <br />Sodium <br />Thallium <br />Uranium <br />Zinc <br />Sample ID: LFB <br />Antimony <br />Calcium <br />Copper <br />Iron <br />Magnesium <br />Manganese <br />Molybdenum <br />Potassium <br />Silver <br />Sodium <br />Thallium <br />Uranium <br />Zinc <br />Qualifiers: <br />RL - Analyte reporting limit. <br />ND - Not detected at the reporting limit. <br />www.energylab.com <br />Analytical &oh= Shut 7952 <br />i <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />13 Sample Matrix Spike Duplicate <br />18.2 mg /L <br />0.0194 mg /L <br />74.5 mg /L 1.0 <br />0.0532 mg /L 0.0010 106 <br />0.0729 mg /L 0.00030 108 <br />0.0523 mg /L 0.010 100 <br />13 Method Blank <br />0.0010 mg /L 0.0002 <br />ND mg /L 0.004 <br />ND mg /L 6E -05 <br />0.0008 mg /L 0.0001 <br />ND mg /L 0.001 <br />ND mg /L 2E -05 <br />0.0002 mg /L 8E -05 <br />0.03 mg /L 0.007 <br />0.0001 mg /L 8E -05 <br />0.09 mg /L 0.004 <br />4E -05 mg /L 2E -05 <br />2E -05 mg /L 8E -06 <br />ND mg /L 0.0001 <br />13 Laboratory Fortified Blank <br />0.0526 mg /L 0.0010 103 <br />12.6 mg /L 0.12 101 <br />0.0546 mg /L 0.0010 109 <br />1.33 mg /L 0.012 106 <br />12.6 mg /L 0.12 101 <br />0.0532 mg /L 0.0010 106 <br />0.0531 mg /L 0.0010 106 <br />12.8 mg /L 0.12 102 <br />0.0209 mg /L 0.0010 104 <br />12.6 mg /L 0.12 100 <br />0.0537 mg /L 0.0010 107 <br />0.0529 mg /L 0.00030 106 <br />0.0556 mg /L 0.0010 111 <br />Helena, MT 877- 472 -0711 • Billings, MT 800 - 735 -4489 • Casper, WY 888 - 235 -0515 <br />Gillette, WY 866- 686 -7175 • Rapid City, SD 888- 672 -1225 • College Station, TX 888 -690 -2218 <br />Report Date: 08/10/11 <br />Work Order: C11070522 <br />RL %REC Low Limit High Limit RPD RPDLimit Qual <br />1.0 107 <br />0.010 97 <br />Run: ICPMS4- C_110721 A <br />70 130 4.0 <br />70 130 4.7 <br />70 130 1.8 <br />70 130 3.0 <br />70 130 1.5 <br />70 130 1.8 <br />Run: ICPMS4- C_110721 A <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />85 115 <br />Batch: R148417A <br />07/22/11 05:05 <br />20 <br />20 <br />20 A <br />20 <br />20 <br />20 <br />Run: ICPMS4-C_110721A 07/21/11 17:01 <br />Page 15 of 28 <br />07/21/11 17:08 <br />A - The analyte level was greater than four times the spike level. In <br />accordance with the method % recovery is not calculated. <br />MDC - Minimum detectable concentration <br />