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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />• <br />• <br />Matheson Mining Consultants <br />Project ID: COALDALE GYPSUM <br />Sample ID: HOLO1 <br />Wet Chemistry <br />Parameter � � <br />EP Metho <br />Acidity as CaCO3 <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Coliforms, fecal <br />Conductivity @25C <br />Fluoride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Nitrogen, ammonia <br />pH (lab) <br />pH <br />pH measured at <br />Residue, Filterable <br />(TDS) @180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measured/calculated) <br />REPIN.02.06.05.01 <br />SM2310B - Titration <br />SM2320B - Titration <br />Calculation <br />325.2 / SM4500CI -E <br />SM9222D - Membrane Filter <br />120.1 / SM2510B <br />SM4500F -C <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 0.17 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />M350.1 - Automated Phenate <br />150.1 / SM4500H+ B <br />160.1 / SM2540C <br />USGS - 11738 -78 <br />375.4 - Turbidimetric <br />Calculation <br />Calculation <br />U mg /L <br />179 mg /L <br />U mg /L <br />U mg /L <br />179 mg /L <br />0.3 <br />30.8 meq /L <br />31.0 meq /L <br />94 mg /L <br />0 * #/100m1 <br />2540 umhos /cm <br />0.2 B * mg /L <br />1080 mg /L <br />0.17 <br />8.0 <br />24.0 <br />2100 <br />2.83 <br />1170 <br />1950 <br />1.08 <br />UH <br />U <br />H <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />units <br />C <br />mg /L <br />mg /L <br />mg /L <br />norgan c Analytical' <br />R esults <br />L68214 -04 <br />03/17/08 12:45 <br />03118108 <br />Ground Water <br />2 10 03/27/08 14:49 ear <br />2 20 03/20/08 0:00 ear /cas <br />2 20 03/20/08 0:00 ear /cas <br />2 20 03/20/08 0:00 ear /cas <br />2 20 03/20/08 0:00 ear /cas <br />04/03/08 0:00 calc <br />0.1 0.5 04/03/08 0:00 calc <br />0.1 0.5 04/03/08 0:00 calc <br />1 5 03/27/08 14:24 aml <br />1 5 03/18/08 12:22 cas <br />1 10 03/20/08 1:26 ear /cas <br />0.1 0.5 03/25/08 17:07 cas <br />1 7 04/03/08 0:00 calc <br />03/19/08 10:21 mis <br />03/18/08 18:08 mis <br />0.02 0.1 04/03/08 0:00 calc <br />0.02 0.1 03/18/08 19:46 pjb <br />0.01 0.05 04/01/08 20:46 ccp <br />0.05 0.5 03/25/08 21:37 pjb <br />0.1 0.1 03/20/08 0:00 ear /cas <br />0.1 0.1 03/20/08 0:00 ear /cas <br />10 20 03/21/08 15:09 cas <br />0.03 0.15 04/03/08 0:00 calc <br />50 300 03/28/08 10:13 aml <br />10 50 04/03/08 0:00 calc <br />04/03/08 0:00 calc <br />* Please refer to Qualifier Reports for details. <br />L68214: Page 9 of 51 <br />