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• <br />• <br />ACZ Laboratories, Inc. <br />110 2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Matheson Mining Consultants <br />PARAMETER <br />L68757 - WG243636 Arsenic, dissolved <br />WG243251 Iron, dissolved <br />WG243341 Iron, total <br />WG243251 Manganese, dissolved <br />WG243204 Mercury, dissolved <br />WG243618 Nickel, dissolved <br />WG243431 Acidity as CaCO3 <br />WG243540 Coliforms, fecal <br />REPAD.15.06.05.01 <br />norg <br />Q <br />ACZ Project ID: L68757 <br />DESCRIPTION <br />Ex =ende <br />0 <br />M200.7 ICP QA Sample container with preservation type specified by the <br />method was not available for analysis. Alternate sample <br />container was used. <br />M200.7 ICP M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />M200.7 ICP M3 The spike recovery value is unusable since the analyte <br />concentration in the sample is disproportionate to the spike <br />level. The recovery of the associated control sample (LCS <br />or LFB) was acceptable. <br />M200.7 ICP MA Recovery for either the spike or spike duplicate was outside <br />of the acceptance limits; the RPD was within the <br />acceptance limits. <br />M245.1 CVAA MA Recovery for either the spike or spike duplicate was outside <br />of the acceptance limits; the RPD was within the <br />acceptance limits. <br />M200.7 ICP QA Sample container with preservation type specified by the <br />method was not available for analysis. Alternate sample <br />container was used. <br />SM2310B - Titration RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />SM9222D - Membrane Filter HE Analysis performed past holding time. Method holding time <br />is less than or equal to 7 days and sample was received <br />with less than half of the holding time remaining (refer to <br />item C5 of ACZ's Terms & Conditions). <br />WG243373 Fluoride SM4500F -C RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG243278 Nitrate /Nitrite as N, dissolved M353.2 - Automated Cadmium HC Initial analysis within holding time. Reanalysis was past <br />Reduction holding time, which was required due to a QC failure during <br />the initial analysis. <br />M353.2 - Automated Cadmium M1 Matrix spike recovery was high, the recovery of the <br />Reduction associated control sample (LCS or LFB) was acceptable. <br />Nitrite as N, dissolved M353.2 - Automated Cadmium HC Initial analysis within holding time. Reanalysis was past <br />Reduction holding time, which was required due to a QC failure during <br />the initial analysis. <br />M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br />Reduction validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG243207 Nitrogen, ammonia M350.1 - Automated Phenate RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />WG243195 Sulfate 375.4 - Turbidimetric M2 Matrix spike recovery was low, the recovery of the <br />associated control sample (LCS or LFB) was acceptable. <br />Page 8 of 16 <br />