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ENERGY <br />LAHOFHA7 ONIL $ <br />Method: E200.7 <br />Sample ID: MB -29636 <br />Iron <br />Client: Cotter Corporation <br />Project: Schwartz GW 4/15/11 S25714 <br />Sample ID: LCS3 -29636 <br />Iron <br />Laboratory Control Sample <br />2.74 mg /L <br />Sample ID: C11040633- 001AMS3 Sample Matrix Spike <br />Iron <br />2.69 mg /L <br />Sample ID: 011040633- 001AMSD Sample Matrix Spike Duplicate <br />Iron <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energyfab.wm <br />AMarest.e. 7152 <br />Method Blank <br />ND mg /L <br />2.70 mg /L <br />Helena, Mr 877- 472 -071 t • Billings, MT 800 - 735 -4489 • Casper, WY 888- 235 -0515 <br />Gillette, WY 866- 686 -7175 • Rapid City, SD 888 -672 -1225 • College Station, IX 888 -680 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />Analyte <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Run: ICP2- C_110426A <br />0.030 <br />Run: ICP2- C_110426A <br />0.030 110 85 115 <br />Run: ICP2- C_110426A <br />0.030 108 70 130 <br />Run: ICP2- C_110426A 04/26/11 15:07 <br />0.030 108 70 130 0.4 20 <br />Method: E200.7 <br />Sample ID: MB- 110426A 6 Method Blank Run: ICP2-C_110426A <br />Aluminum <br />ND mg /L 0.20 <br />Calcium ND mg /L 0.20 <br />Iron ND mg /L 0.030 <br />Magnesium ND mg /L 0.10 <br />Potassium ND mg /L 0.10 <br />Sodium ND mg /L 0.40 <br />Sample ID: LFB- 110426A 6 Laboratory Fortified Blank Run: ICP2- C_110426A 04/26/11 10:24 <br />Aluminum 0.931 mg /L 0.10 93 85 115 <br />Calcium 48.3 mg /L 0.50 97 85 115 <br />Iron 0.984 mg /L 0.030 98 85 115 <br />Magnesium 50.3 mg /L 0.50 101 85 115 <br />Potassium 48.0 mg /L 0.50 96 85 115 <br />Sodium 48.6 mg /L 0.50 97 85 115 <br />Sample ID: C11030715- 005BMS2 6 Sample Matrix Spike Run: ICP2- C_110426A 04/26/11 12:49 <br />Aluminum 2.08 mg /L 0.10 97 70 130 <br />Calcium 114 mg /L 1.0 98 70 130 <br />Iron 2.12 mg /L 0.030 98 70 130 <br />Magnesium 108 mg /L 1.0 99 70 130 <br />Potassium 96.3 mg /L 1.0 84 70 130 <br />Sodium 147 mg /L 1.0 100 70 130 <br />Sample ID: C11030715- 005BMSD 6 Sample Matrix Spike Duplicate Run: ICP2- C_110426A 04/26/11 12:53 <br />Aluminum 2.06 mg /L 0.10 96 70 130 1.3 20 <br />Calcium 112 mg /L 1.0 96 70 130 2.2 20 <br />Iron 2.12 mg /L 0.030 98 70 130 0.3 20 <br />Magnesium 107 mg /L 1.0 98 70 130 0.9 20 <br />Potassium 95.1 mg /L 1.0 83 70 130 1.2 20 <br />Sodium 145 mg /L 1.0 98 70 130 1.1 20 <br />ND - Not detected at the reporting limit. <br />Report Date: 05/17/11 <br />Work Order: C11040550 <br />Page 7 of 19 <br />Batch: 29636 <br />04/26/11 14:39 <br />04/26/11 14:43 <br />04/26/11 15:03 <br />Batch: R145219 <br />04/26/11 10:19 <br />