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ENERGY <br />AHOF7AI OHIF_S <br />Client: Cotter Corporation <br />Project: Schwartz GW 4/20/11 S25759- S25760 <br />Analyte <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.8 <br />Sample ID: MB -29656 <br />Aluminum <br />Antimony <br />Arsenic <br />Copper <br />Lead <br />Manganese <br />Thallium <br />Zinc <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />mintenerrfiab.cOM <br />Enema atria 7952 <br />8 Method Blank <br />ND mg /L <br />0.0003 mg /L <br />0.0005 mg /L <br />0.0005 mg /L <br />ND mg /L <br />0.002 mg /L <br />0.0002 mg /L <br />0.006 mg /L <br />Helena, MT 877- 472 -0711 • Billings, MT 800 -735 -4489 • Casper, WY 888 - 235 -0515 <br />Gillette, WY 866- 686 -7175 • Rapid City, SD 888 - 672 -1225 • College Station, TX 888 -690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />0.01 <br />0.0002 <br />0.0003 <br />0.0005 <br />5E -05 <br />9E -05 <br />5E -05 <br />0.001 <br />Run: ICPMS2 -C 110427A <br />Sample ID: LCS3 - 29656 8 Laboratory Control Sample Run: ICPMS2- C_110427A 04/28/11 02:43 <br />Aluminum 2.24 mg /L 0.10 90 85 115 <br />Antimony 0.583 mg /L 0.050 117 85 115 S <br />Arsenic 0.521 mg /L 0.0010 104 85 115 <br />Copper 0.489 mg /L 0.010 98 85 115 <br />Lead 0.543 mg /L 0.050 109 85 115 <br />Manganese 2.54 mg /L 0.010 102 85 115 <br />Thallium 0.532 mg /L 0.10 106 85 115 <br />Zinc 0.507 mg /L 0.010 100 85 115 <br />- Response is above standard QA limit. This could indicate a high bias for the sample results. Since there were no detectable analyte responses, and the remainder of the <br />run QA is within acceptance range, this batch is approved. <br />Sample ID: C11040686 006AMS3 8 Sample Matrix Spike Run: ICPMS2- C_110427A 04/28/11 04:38 <br />Aluminum 2.19 mg /L 0.10 87 70 130 <br />Antimony 0.552 mg /L 0.050 110 70 130 <br />Arsenic 0.526 mg /L 0.0010 105 70 130 <br />Copper 0.464 mg /L 0.010 92 70 130 <br />Lead 0.544 mg /L 0.050 109 70 130 <br />Manganese 2.66 mg /L 0.010 101 70 130 <br />Thallium 0.545 mg /L 0.10 109 70 130 <br />Zinc 0.453 mg /L 0.010 88 70 130 <br />Sample ID: C11040686 006AMSD 8 Sample Matrix Spike Duplicate Run: ICPMS2- C_110427A 04/28/11 05:12 <br />Aluminum 2.30 mg /L 0.10 91 70 130 4.7 20 <br />Antimony 0.578 mg /L 0.050 116 70 130 4.6 20 <br />Arsenic 0.513 mg /L 0.0010 102 70 130 2.7 20 <br />Copper 0.458 mg /L 0.010 91 70 130 1.2 20 <br />Lead 0.559 mg /L 0.050 112 70 130 2.7 20 <br />Manganese 2.70 mg /L 0.010 102 70 130 1.2 20 <br />Thallium 0.540 mg /L 0.10 108 70 130 0.9 20 <br />Zinc 0.446 mg /L 0.010 87 70 130 1.5 20 <br />ND - Not detected at the reporting limit. <br />S - Spike recovery outside of advisory limits. <br />Report Date: 05/19/11 <br />Work Order: C11040679 <br />Page 10 of 23 <br />Batch: 29656 <br />04/28/11 02:36 <br />