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ENERGY <br />L AAORATORIES <br />Method: E300.0 <br />Sample ID: ICV- 110613 <br />Chloride <br />Sulfate <br />Sample ID: LFB- 110613 <br />Chloride <br />Sulfate <br />Qualifiers: <br />RL - Analyte reporting limit. <br />MDC - Minimum detectable concentration <br />www.energyiab.com <br />Aaa►rt�a lEatariaSwann <br />Client: Cotter Corporation <br />Project: Schwartz SW 6/1/11 S25340- S25347 <br />2 Laboratory Fortified Blank <br />9.75 mg /L <br />38.8 mg /L <br />Helena, MT I777-472-0711 • Billings, MT B00- 7354489 • Casper, WY 888- 235 -0515 <br />Gillette, WY 86B -686 -7175 • Rapid City, Su 888- 872 -1225 • College Station, T% 888 -690 -2218 <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />2 Initial Calibration Verification Standard <br />9.86 mg /L 1.0 99 90 110 <br />38.7 mg /L 1.0 97 90 110 <br />Method: E300.0 <br />Sample ID: ICB- 110613 2 Method Blank <br />Chloride ND mg /L 3.0 <br />Sulfate ND mg /L 5.0 <br />Run: IC2- C_110613A <br />ND - Not detected at the reporting limit. <br />S - Spike recovery outside of advisory limits. <br />Report Date: 07/12/11 <br />Work Order: C11060117 <br />Analyte Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Analytical Run: IC2- C_110613A <br />06/13/11 14:55 <br />Batch: R146932 <br />06/13/11 15:11 <br />Run: IC2- C_110613A 06/13/11 15:26 <br />1.0 97 90 110 <br />1.0 96 90 110 <br />Sample ID: C11060172- 002AMS 2 Sample Matrix Spike Run: IC2- C_110613A 06/13/11 17:29 <br />Chloride 100 mg /L 2.0 98 80 120 <br />Sulfate 1650 mg /L 8.0 72 80 120 S <br />- Matrix spike recoveries outside the acceptance range are considered matrix - related. <br />Sample ID: C11060172- 002AMSD 2 Sample Matrix Spike Duplicate Run: IC2- C_110613A 06/13/11 17:45 <br />Chloride 101 mg /L 2.0 99 80 120 0.9 10 <br />Sulfate 1630 mg /L 8.0 69 80 120 0.7 10 S <br />- Matrix spike recoveries outside the acceptance range are considered matrix - related. <br />Page 22 of 38 <br />