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ENERGY <br />LABORATORIES <br />Qualifiers: <br />1' <br />Client: Cotter Corporation <br />Project: Schwartz SW 6/15/11 S25772- S25774 <br />www.eaer®riab.com Helena, MT 877 -472 -0711 • Billings MT 8 735-4489 • Casper, WY 888 - 235 -0515 <br />s e lit Gillette, W 806 - 686 -7175 • Repid City SO 886 672;1 • College Station, IX 888 - 690 -2218 <br />Analyte <br />Count Result Units RL %REC Low Limit High Limit RPD RPDLimit Qual <br />Method: E200.8 <br />Sample ID: C11060727- 001CMS4 18 Sample Matrix Spike <br />Chromium <br />Copper <br />Iron <br />Lead <br />Magnesium <br />Manganese <br />Molybdenum <br />Potassium <br />Silver <br />Sodium <br />Thallium <br />Uranium <br />Zinc <br />QA/QC Summary Report <br />Prepared by Casper, WY Branch <br />0.0522 mg /L <br />0.0510 mg /L <br />1.32 mg /L <br />0.0523 mg /L <br />21.6 mg /L <br />0.0669 mg /L <br />0.0526 mg /L <br />20.4 mg /L <br />0.0157 mg /L <br />43.1 mg /L <br />0.0520 mg /L <br />0.0505 mg /L <br />0.0541 mg /L <br />Run: ICPMS4- C_110621 A <br />0.050 104 70 130 <br />0.010 102 70 130 <br />0.030 102 70 130 <br />0.050 105 70 130 <br />1.0 97 70 130 <br />0.010 101 70 130 <br />0.0010 103 70 130 <br />1.0 99 70 130 <br />0.010 78 70 130 <br />1.0 94 70 130 <br />0.0010 104 70 130 <br />0.00030 101 70 130 <br />0.010 105 70 130 <br />Report Date: 08/03/11 <br />Work Order: C11060712 <br />Batch: R147207A <br />06/22/11 12:59 <br />Sample ID: C11060727- 001CMSD 18 Sample Matrix Spike Duplicate Run: ICPMS4- C_110621A 06/22/11 13:06 <br />Aluminum 0.0575 mg /L 0.0010 99 70 130 0.0 20 <br />Antimony 0.0574 mg /L 0.050 115 70 130 2.6 20 <br />Arsenic 0.0536 mg /L 0.0010 107 70 130 2.4 20 <br />Boron 0.110 mg /L 0.10 104 70 130 5.7 20 <br />Calcium 68.3 mg /L 1.0 70 130 1.3 20 A <br />Chromium 0.0530 mg /L 0.050 106 70 130 1.5 20 <br />Copper 0.0516 mg /L 0.010 103 70 130 1.3 20 <br />Iron 1.35 mg /L 0.030 104 70 130 1.9 20 <br />Lead 0.0530 mg /L 0.050 106 70 130 1.4 20 <br />Magnesium 21.8 mg /L 1.0 99 70 130 1.1 20 <br />Manganese 0.0674 mg /L 0.010 102 70 130 0.8 20 <br />Molybdenum 0.0546 mg /L 0.0010 107 70 130 3.7 20 <br />Potassium 20.9 mg /L 1.0 103 70 130 2.4 20 <br />Silver 0.0175 mg /L 0.010 88 70 130 11 20 <br />Sodium 44.0 mg /L 1.0 101 70 130 1.9 20 <br />Thallium 0.0531 mg /L 0.0010 106 70 130 2.2 20 <br />Uranium 0.0517 mg /L 0.00030 103 70 130 2.3 20 <br />Zinc 0.0538 mg /L 0.010 105 70 130 0.6 20 <br />RL - Analyte reporting limit. A - The analyte level was greater than four times the spike level. In <br />accordance with the method % recovery is not calculated. <br />ND - Not detected at the reporting limit. MDC - Minimum detectable concentration <br />Page 15 of 29 <br />