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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334 -5493 <br />Kerr Coal Company <br />Project ID: <br />Sample ID: <br />Field Data <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />Conductivity (Field) <br />pH (Field) <br />Temperature (Field) <br />Metals Analysis <br />Parameter <br />EPA Method <br />Result Qua! XQ Units MDL PQL <br />Date Analyst <br />Calcium, dissolved <br />Iron, dissolved <br />Magnesium, dissolved <br />Manganese, dissolved <br />Potassium, dissolved <br />Sodium, dissolved <br />Wet Chemistry <br />Alkalinity as CaCO3 <br />Bicarbonate as <br />CaCO3 <br />Carbonate as CaCO3 <br />Hydroxide as CaCO3 <br />Total Alkalinity <br />Cation -Anion Balance <br />Cation -Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride <br />Hardness as CaCO3 <br />Lab Filtration <br />Lab Filtration & <br />Acidification <br />Nitrate as N, dissolved <br />Nitrate /Nitrite as N, <br />dissolved <br />Nitrite as N, dissolved <br />Residue, Filterable <br />(TDS) @180C <br />Sodium Absorption <br />Ratio in Water <br />Sulfate <br />TDS (calculated) <br />TDS (ratio - <br />measu red /calculated ) <br />REPIN.02.06.05.01 <br />AP -1 <br />Field Measurement <br />Field Measurement <br />Field Measurement <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />M200.7 ICP <br />SM2320B - Titration <br />Calculation <br />SM4500CI -E <br />SM2340B - Calculation <br />SM 3030 B <br />SM 3030 B <br />Calculation: NO3NO2 minus NO2 <br />M353.2 - Automated Cadmium <br />Reduction <br />M353.2 - Automated Cadmium <br />Reduction <br />SM2540C <br />USGS - 11738 -78 <br />SM4500 SO4 -D <br />Calculation <br />Calculation <br />600 <br />8.0 <br />13.0 <br />48.5 <br />0.16 <br />37.2 <br />0.495 <br />1.2 B <br />21.4 <br />Parameter <br />EPA Method <br />Result Qual XQ Units MDL PQL <br />Date Analyst <br />289 <br />10 <br />299 <br />0.0 <br />6.4 <br />6.4 <br />2 <br />274 <br />0.03 <br />0.04 <br />0.01 <br />20 <br />315 <br />0.98 <br />B <br />U <br />B <br />B <br />B <br />B <br />B <br />umhos /cm <br />units <br />C <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />mg /L <br />meq /L <br />meq /L <br />mg /L <br />mg /L <br />ACZ Sample ID: <br />Date Sampled: <br />Date Received: <br />Sample Matrix: <br />0.2 1 05/21/10 11:19 aeh <br />0.02 0.05 05/21/10 11:19 aeh <br />0.2 1 05/21/10 11:19 aeh <br />0.005 0.03 05/21/10 11:19 aeh <br />0.3 2 05/21/1011:19 aeh <br />0.3 2 05/21/1011:19 aeh <br />mg /L 0.02 0.1 05/26/10 12:01 calc <br />mg /L 0.02 0.1 05/18/10 22:40 pjb <br />mg /L 0.01 0.05 05/18/10 22:40 pjb <br />310 mg /L 10 20 05/19/10 11:29 jjc <br />0.56 0.03 0.15 05/26/10 12:01 calc <br />mg /L 10 50 <br />mg /L 10 50 <br />Inorganic Analytical <br />Results <br />L82183 -01 <br />05/17/10 14:00 <br />05/18/10 <br />Ground Water <br />05/17/10 14:00 <br />05/17/10 14:00 <br />05/17/10 14:00 <br />2 20 05/21/10 0:00 <br />2 20 05/21/10 0:00 <br />2 20 05/21/10 0:00 <br />05/24/10 12:12 <br />05/26/10 12:01 <br />05/26/10 12:01 <br />Page 2 of 10 <br />im <br />jm <br />jm <br />2 20 05/21/10 0:00 jjc <br />jjc <br />jjc <br />jjc <br />05/26/10 12:01 calc <br />0.1 0.5 05/26/10 12:01 calc <br />0.1 0.5 05/26/10 12:01 calc <br />1 5 05/19/10 15:59 aml <br />1 7 05/26/10 12:01 calc <br />05/18/10 14:24 jlf <br />05/19/10 3:00 cra <br />fhb <br />calc <br />calc <br />* Please refer to Qualifier Reports for details. <br />