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032 <br />Work Order: 09-8452 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 21355 <br />Sample ID: 09-8452-01BMS SampType: MS TestCode: 200.8_D Run ID: ICPMS 091031A Prep Date: 10129/2009 Units: mg/L <br />Client ID: MW-002 Batch ID: 21355 TestNo: E200,8 FilelD: 103009AQ109-8452.01BMS.0 Analysis Date: 10/30/2009 SegNo: 931355 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit Highlimit RPD Ref Val %RPD RPDLimit Qual <br />Lead 0.1297 0.00100 0.125 0.000185 104 70 130 0 0 <br />Selenium 0.05727 0.00200 0.05 0.00371 107 70 130 0 0 <br />Silver 0.121 0.000200 0.125 0 96.8 70 130 0 0 <br />Thallium 0.118 0,00100 0.125 0 94.4 70 130 0 0 <br />Sample ID: 09-8452-01BMSD SampType: MSD TestCode: 200.8_D Run ID: ICPMS 091031A Prep Date: 10/29/2009 Units: mg/L <br />Client ID: MW-002 Batch ID: 21355 TestNo: E200.8 FilelD: 103009AQ109-8452.01112IMS0. Analysis Date: 10/30/2009 SegNo: 931358 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimlt RPD Ref Val %RPD RPDLimit Qual <br />Antlmony 0.1187 0.00200 0.125 0.00033 95 70 130 0,1208 1.70 20 <br />Arsenic 0.2704 0.00200 0.25 0.001695 108 70 130 0.2745 1.48 20 <br />Cadmium 0.02433 0.000500 0.025 0 97.3 70 130 0,02472 1.57 20 <br />Copper 0.4663 0.0100 0.5 0,0034 93.3 70 130 0.4785 2.60 20 <br />Lead 0.1281 0.00100 0.125 0.000185 102 70 130 0,1297 1.25 20 <br />Selenium 0.05943 0.00200 0.05 0.00371 111 70 130 0.05727 3,70 20 <br />Silver 0.1213 0.000200 0.125 0 97.1 70 130 0.121 0.281 20 <br />Thallium 0.1164 0.00100 0,125 0 94.8 70 130 0.118 0,419 20 <br />Qualifiers: U - Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br />i J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br />S - Spike Recovery outside acceptance limits H - Prep or analytical holding time exceeded <br />E - Extrapolated value, value exceeds calibration range. X - See case narrative <br />i