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/ Lid.' Laboratories, Inc. <br />9773 I)nwnhw nriva Staamhnat Snrinas. CO 80487 (8001 <br />Natural Soda, Inc. ACZ Sample ID: L85860-02 <br />Project ID: Date Sampled: 12195110 09:30 <br />Sample ID: B-SOLN Date Received: 12116110 <br />Sample Matrix: Waste Water <br />Inorganic Prep <br />Phosphorus, total M365.1 - Auto Ascorbic Acid 12/21/10 14:44 Ihb <br />Digestion <br />Total Hot Plate M200.2 ICP-MS 12/22/10 20:10 scp <br />Digestion <br />Total Hot Plate M200.2 ICP * 12/21/10 17:15 jjc <br />Digestion <br />Metals Analysis <br />Parameter EPA i <br />Aluminum, total M200.7 ICP 0.6 B mg/L 0.6 3 12/27/10 19:10 jjc <br />Antimony, total M200.8 ICP-MS U mg/L 0.008 0.04 12/27/10 20:26 msh <br />Arsenic, total M200.7 ICP U mg/L 6 30 01/07/11 12:08 jjc <br />Barium, total M200.7 ICP 0.66 mg/L 0.06 0.3 12/27/10 19:10 jjc <br />Beryllium, total M200.7 ICP U mg/L 0.2 1 01/04/11 16:27 jjc <br />Boron, total M200.7 ICP 59.8 mg/L 0.2 1 12/27/10 19:10 jjc <br />Cadmium, total M200.7 ICP U mg/L 0.1 0.3 12/27/10 19:10 jjc <br />Calcium, total M200.7 ICP U mg/L 20 100 12/31/10 1:53 jjc <br />Chromium, total M200.7 ICP U mg/L 0.2 1 12/27/10 19:10 jjc <br />Cobalt, total M200.7 ICP U mg/L 0.2 1 12/27/10 19:10 jjc <br />Copper, total M200.7 ICP U mg/L 0.2 1 12/27/10 19:10 jjc <br />Iron, total M200.7 ICP U mg/L 0.4 1 12/27/10 19:10 jjc <br />Lead, total M200.7 ICP U mg/L 0.8 4 12/27/10 19:10 jjc <br />Lithium, total M200.7 ICP 1.0 B mg/L 0.4 2 12/27/10 19:10 jjc <br />Magnesium, total M200.7 ICP U mg/L 4 20 12/27/10 19:10 jjc <br />Manganese, total M200.7 ICP U mg/L 0.1 0.5 12/27/10 19:10 jjc <br />Mercury, total M245.1 CVAA U mg/L 0.001 0.005 12/29/10 12:43 erf <br />Molybdenum, total M200.7 ICP U mg/L 0.2 1 12/27/10 19:10 jjc <br />Nickel, total M200.7 ICP U mg/L 0.2 1 12/27/10 19:10 jjc <br />Potassium, total M200.7 ICP 76 mg/L 6 30 12/27/10 19:10 jjc <br />Selenium, total M200.7 ICP U mg/L 6 30 12131/10 1:53 jjc <br />Silica, total M200.7 ICP 80 B mg/L 40 200 12131/10 1:53 jjc <br />Silver, total M200.7 ICP U mg/L 0.2 0.5 12/27/10 19:10 jjc <br />Sodium, total M200.7 ICP 24700 mg/L 30 200 12/31/10 1:53 jjc <br />Strontium, total M200.7 ICP U mg/L 0.2 1 12/27/10 19:10 jjc <br />Thallium, total M200.7 ICP U * mg/L 6 20 12/27/10 19:10 jjc <br />Uranium, total M200.8 ICP-MS 0.322 mg/L 0.002 0.01 12/27/10 20:26 msh <br />Vanadium, total M200.7 ICP U mg/L 0.1 0.5 12/27/10 19:10 jjc <br />Zinc, total M200.7 ICP U mg/L 0.2 1 12/27/10 19:10 jjc <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 4 of 40 <br />