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ARL iL Laboratories, Inc. <br />977Q r)-hill rbiva Rtaamhnat.Snrinnc en R04R7 (800) <br />Inorganic Prep <br />Parameter EPA Method Result Qual KQ :1 n its 11113L PQL <br />Phosphorus, total M365.1 - Auto Ascorbic Acid 12/21/10 14:27 Ihb <br />Digestion <br />Total Hot Plate M200.2 ICP 12/20/10 18:42 aeb <br />Digestion <br />Total Hot Plate M200.2 ICP-MS 12/22/10 19:50 scp <br />Digestion <br />Metals Analysis <br /> <br />Aluminum, total M200.7 ICP 0.8 B mg/L 0.6 3 12/27/10 22:24 aeb <br />Antimony, total M200.8 ICP-MS U mg/L 0.008 0.04 12/27/10 20:22 msh <br />Arsenic, total M200.7 ICP U mg/L 3 20 12/30110 17:33 aeb <br />Barium, total M200.7 ICP 0.76 mg/L 0.06 0.3 12127/10 22:24 aeb <br />Beryllium, total M200.7 ICP U mg/L 0.1 0.5 12/29/10 14:15 aeb <br />Boron, total M200.7 ICP 38.4 mg/L 0.5 3 12/28/10 16:53 jjc <br />Cadmium, total M200.7 ICP U mg/L 0.1 0.3 12/27/10 22:24 aeb <br />Calcium, total M200.7 ICP 6 B mg/L 4 20 12127/10 22:24 aeb <br />Chromium, total M200.7 ICP U mg/L 0.2 1 12/27/10 22:24 aeb <br />Cobalt, total M200.7 ICP U mg/L 0.2 1 12/27/10 22:24 aeb <br />Copper, total M200.7 ICP U mg/L 0.2 1 12/27/10 22:24 aeb <br />Iron, total M200.7 ICP U mg/L 0.4 1 12127/10 22:24 aeb <br />Lead, total M200.7 ICP U mg/L 0.8 4 12/27/10 22:24 aeb <br />Lithium, total M200.7 ICP 1.0 B mg/L 0.4 2 12/27110 22:24 aeb <br />Magnesium, total M200.7 ICP U mg/L 4 20 12/27/10 22:24 aeb <br />Manganese, total M200.7 ICP U mg/L 0.1 0.5 12/27/10 22:24 aeb <br />Mercury, total M245.1 CVAA U mg/L 0.001 0.005 12/29/10 12:41 erf <br />Molybdenum, total M200.7 ICP U mg/L 0.2 1 12/27/10 22:24 aeb <br />Nickel, total M200.7 ICP U mg/L 0.2 1 12/27/10 22:24 aeb <br />Potassium, total M200.7 ICP 76 mg/L 6 30 12/27/10 22:24 aeb <br />Selenium, total M200.7 ICP U mg/L 3 20 12/28/10 16:53 jjc <br />Silica, total M200.7 ICP 70 B mg/L 20 100 12/28/10 16:53 jjc <br />Silver, total M200.7 ICP U mg/L 0.2 0.5 12/27/10 22:24 aeb <br />Sodium, total M200.7 ICP 18200 mg/L 20 80 12/28110 16:53 jjc <br />Strontium, total M200.7 ICP U mg/L 0.2 1 12/27/10 22:24 aeb <br />Thallium, total M200.7 ICP U mg/L 6 20 12/27/10 22:24 aeb <br />Uranium, total M200.8 ICP-MS 0.321 mg/L 0.002 0.01 12/27/10 20:22 msh <br />Vanadium, total M200.7 ICP U mg/L 0.3 1 - 12/28/10 16:53 jjc <br />Zinc, total M200.7 ICP U mg/L 0.2 1 12/27/10 22:24 aeb <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for details. <br />Page 2 of 40 <br />Natural Soda, Inc. ACZ Sample ID: L85860-01 <br />Project ID: Date Sampled: 12115110 09:00 <br />Sample ID: P-SOLN Date Received: 12116110 <br />Sample Matrix: Waste Water