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<br />i'y} <br />Work Order: -6 - ?r16? Sample: D 4 Tech: Gs xl -" <br />Date:A/- / Client: Matrix: Comments: <br />Determination of extraction fluid: <br />5g sample + 96.5 mL H2O, stir 5 minutes .................... <br />Is pH <5.00? <br />Yes Use extraction fluid #1. <br />No d Add 3.5 mL 1 N HCI, heat to 50°C far 10 m <br />...................................................................................... <br />Is pH <5.00? <br />Yes r/ Use extraction fluid #I. <br />No Use extraction fluid 42. <br />Net weight of sample-7 X 20 = mLs of extr <br />Sample required extraction fluid # L with pH of <br />(# 1 pH 4.88 to 4.98, #2 pH 2.83 <br />Time rotation started 4! 9opm?4topped-' <br />po <br />.......................Initial pH c.'O <br />cool to room temp. 6 :7 <br />..............Check pH liv--l <br />ion fluid 24M mLs. <br /> <br />7 ^V.......Final PH 9S -q0 <br />Work Order: Sample: <br />Date: Client: Matrix: <br />Comments: <br />Determination of extraction fluid: <br />Sg sample .+ 96.5 mL H2O, stir 5 minutes ...........................................Initial pH <br />Is pH <5.00? <br />Yes Use extraction fluid #1. <br />No Add 3.5 mL IN HCI, heat to 50°C for 10 min., cool to room temp. <br />.........................................................................................................Check pg______ <br />Is pH <5.00? <br />Yes Use extraction fluid #1. <br />No Use extraction fluid #2. <br />Net weight of sample R X 20 = mLs of extraction fluid mLs. <br />Sample required extraction fluid # with pH of i <br />(#I pH 4.88 to 4.98, #2 pH 2.83 to 2.93) <br />Time rotation startedpm Stopped am ...........Final pH <br />• <br />Tech: