2010-08-18_ENFORCEMENT - C1981008

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Client: Walsh Environmental client project Name: New Horizon Mine Client Project Number: 900882.0001,010 Client Sample Number: SS-32A Client Sample Location: New Horizon Mine. 36-60 Sampling Dale : 711512010 Sampling Time: Sample Matrix: Soil Sampler: Edward Analysis Method: •ILP-MS, EPA Methods 6020 /200fip Method: Key Laboratories, Inc. 2479A Riverside Parkway Grand Junction. Colorado 81505-1319 Phone (970) 243-5311 Fax (970) 243-6010 trey Lab #: 10.1030 Work Order 9: 0716101002 Date Received: 07/16/10 Analyst: IV -k Sample Prep: Total, Open Vessel EPA Method 200.6 open Vessel Microwave Dig.lien Thursday, July Date Analyzed: 22, 2010 00:27:22 Wednesday, July 21, 2010 20:14:79 Key Lab.Prep Bntch Sample IDN WI-07208-10- 1030-201X10X Sample Comments: Sample Aliquot lmg]: 1082.1 Prep Au Spike Recovery; 1.013 Prep/Digestion Dr- 46.21 Pass Audit ==>> x TotalDF=» 462.06 WI.07208.10- 0000.01_LMB LMB 1000 0.983 so 500.00 Anaty113 Ion Tlme Me= Man m. • sa""b0I RCRA t.lmrr, Audit Analyte RepoAed Valise Units Method Blank Blank DF MDL ppm PQL ppm Maz ppm I --if Analytes Repotted ICP-Ma' 7 100 Li Lithium mgfKg 600.00 0.25 1 600 IcP.M6' 9 to Be Beryllium mg/Kg < < ` MP-MS' 11 too B Boron mgfKg 600.00 0.5 2 50D CP•Ma- 23 1. Na Sodium mgfKg < < ` IOPMS as In Mg Magnesium mglKg < < < RGP•Ma- 27 1o Al Aluminum mg/Kg IcFMs. as 10 Si SilicOn mgfKg < < < IcP-us• m o I, Phosphorus mgfKg < < < Icp-Ma' 39 no K Potassium mgfKg < < < IcP,ur a1 20 Ca Calcium mg/Kg < ` < MP."- 4a to Ti Titanium mglKg c < c IOp-ma.. 6+ m V Vanandium mgfKg < < < Icp .. sz in Cr 100 Chromium mgfKg ` < < Ic-s- 96 to Mn Manganese mgfKg < < < IU-M9' ee 20 Fe Iron mg/Kg Ia•MS' 59 10 CO Cobalt mgfKg < < < rs-MS• 60 10 Ni Nickel mg/Kg I?• ° in Car Co per mgfKg < c < ICp.M6- 66 10 zn zine mgfKg < Icp ns' 75 fro As 100 Arsemc mgfKg 500.00 0.46 1.8 1000 ICP 31 az 1oc Se 20 x Selenium 0.42 .1 mgfKg < 600.00 0.15 0.6 io00 ,CP.a. as 1m Sr Strontium mglKg 60QOD 0.025 0.1 1000 ICP•MS 93 to Mo Molybdenum mgfKg < < c IGP•119' 1. to Ag 100 Silver mgfKg ` < < 1C.MS• W 1o Cd 20 Cadmium mg1Kg < < < 1cRMS 123 1e Sb Antimony mgfKg < < < +cp.Ms• 137 1m Bit 2000 Barium mg1Kg 500.00 0,03 0.12 1000 ICP.146- non 10 Hg 4 Mercury mgfKg < < < ICPM9' 236 TI Thallium mg ...a' 2N Lead mg/Kg ICKMa' 237 4 ! t? Thorlum mgfKg Uo 0.005 0.D2 500 ICP.Ma• 238 1J-R-(D- mgfKg 500.00 0.006 0.02 500 •Typically, all metals witlr>= 90Ims1 integration time can be reported. Avnilable at customer's request. Notes: LMB = laboratory method blank, M and MD - sample matrix replicates Notes: LCS = spiked laboratory method blank, MS and MSD - spiked sample matrix replicates Notes; Au is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF • Dilution Factor, Notes: MDL = Method Defection Limit, PQL - Primary Qualltltation Limit, MQL= Maximum Quantltation Limit, Notes: c = less than MDL, J = Greater than MDL but less than PQL (4 x MDL), E -Estimated Value because It exceeds the MQL Notes: n.a. = Not Applicable, Blank Space = Not Requested or Not Reported Notes: RCRA TCLP Extract Limits: 8a - 100 ppm; (Cr, As,Ag,Pb] = 6ppm; (Se, Cd] - 1 ppm; Hg = 0.2 ppm Notes: "(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (2000ml.). -EPA SW846 Method 1311, Revision 0, July 1992, Section 1.2: -1f a total analysis of the waste demonstrates that individual analytos are not present in the waste, or that they are present but w such low concentrations that the appropriate regulatory levels could not possibly be exceeded, The TCLP need not be tun' Analyst/ Reviewer ?_s