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Key Laboratories, Inc. <br />Client: Walsh Environmental 7479A Riverside Parkway <br />Client Project Name : New Horizon Mine Grand Junction, Colorado 81505-1319 <br />Client Project Number : 900882.0001.010 Phone (970) 243-5311 Fax (970) 243-6010 <br />Client Sample Number: NHSS-2318 <br />Client Sample Location: Nov Horizon Mine. 24-48 Key Lab:: 10-1019 <br />Sampling Date : 7/15/2010 Work Order g : 0716101002 <br />Sampling Time: <br />Sample Matrix: Soil Data Received: <br />Analyst: 07/16/10 •-^7 <br /> <br />r <br />Sampler: Edward Sample Prep. Tntal, Open Vas.] <br />Analysis Method : •ICP-MS, EPA Methods 6020 /200ttp Method: EPA Method 200.6 Opan Vessel Microwave Digesliaa <br />Wednesday, Wednesday, <br />Date Analyzed: July 21, 2010 July 21, 2010 <br />23:07:06 20:14:39 <br />Key Lab Prep Batch Sample [DN WI-07205.10• WI-07208.10- <br />1019-091XiDX OODO.01_LMB <br />Sample Comments: LMB <br />Sample Aliquot inigi: 1070,6 1000 <br />Prep Au Spike Recovery: 1.006 0.983 <br />Prep/Digestion DF=» 46.70 5o <br />Pass Audit ==>> x Total DF?>> 467.03 500.Do <br />anatya, ton Fa--' aacTU Audit AnalYIa Reported Value Units Method Blank Blank DF MDL ppm PQL ppm Max QL ppm <br />I <<== # Analvtes Reported <br />tcPMS• r tco Li Lithium mg/Kg 500.00 0.25 1 Soo <br />ICP-Ma' 9 ,o Be Beryllium mg1Kg < < < <br />kPUS• " '- B Boron mgfKg 500.00 0.5 2 500 <br />MS• v 1o Na Sodium mg/Kg < < < <br />cP-Ms' 24 1. M Magnesium mg/Kg < e < <br />lcP.eu• V 1. AI Aluminum mg/Kg < < < <br />IC'45. 20 to Si <br />31 10 P SHICDn mg/Kg < < < <br />=-M6' 39 ,o K Potassium mg/Kg < < < <br />IGPMC .. :3 Ca Calcium m01Kg < c < <br />tcPMS• 4e 10 Ti Titanium mg1K9 < < < <br />iMus• 51 10 V Vanandium mg/Kg < < < <br />1-14s' 52 1. Cr 100 Chromium mg1Kg < < c <br />ICp•Ms• 55 16 Mn Manganese mg/Kg < < < <br />CPM6' St 20 Fe Iron mg11(g < < < <br />,CPMS• w 10 Co Cobalt mg/Kg < < < <br />(CPMS• so ,o Ni Nickel mg/Kg c < < <br />1W.Ms• 63 +6 Cu Co er mg/Kg < < < <br />[ -Ma• 66 ,o Zn Zinc mg/Kg < < < <br />,U.Mfi- rs too As 100 Arsenic mglXg 500.00 0.45 1.8 1000 <br />MRS' e2 10 Se 20 x Selenium 0.49 J mglKg < 500.00 0.15 o.s 1000 <br />"P'"'s' Be 100 Sr Strontium mglKg 500.00 0.025 0.1 1000 <br />tcP+as• 1a Mo Molybdenum mglKg < < <br />roPMS• for to Ag IpO Silver mgiKg < c < <br />IGPM3• 111 +o Cd 20 Cadmium mgiKg < < < <br />i-MS• 123 +o Sb Antimony mg/Kg < < c <br />1CP-M6• 131 1oa BA 2000 Barium mglKg 500.00 0.03 0.12 1000 <br />1W.M. 20z 10 H 4 Mcrcur mg/Kg < < < <br />icP-MS• 2. 10 Ti Thallium mg1Kg < < < <br />ICP M6• J04 1o Pb 100 Lead mg/Kg < < < <br />x;P-ars• 232 100 Th Thorium mg/Kg 500.00 0.006 0.02 500 <br />,cP.us• 23e ,oo IJ Uranium mg1Kg 600.00 0.005 0.02 SOD <br /> <br />"Typica9y, ali meIola with>= 901ros)integ tatiau time salt he ,Zparlad. Avntla6le nt customer's reoucsL <br />Notes: LMB = laboratory method blank, M and MD= sample matrix replicates <br />Notes: LCS = spiked laboratory method blank, MS and MSD - spiked sample matrix replicates <br />Notes: Au is spiked as sample prep surrogate and to facilitate analysis of Mercury, OF -Dilution Factor, <br />Notes: MDL = Method Detection Limit, PQL = Primary Quantitation Limit, MQL= Maximum Quantitatton Limit, <br />Notes: < = less than MOIL, J - Greater than MDL but less than PQL (4 x MDL), E- Estimated Value because It exceeds the MQL <br />Notes: n.a. = Not Applicable, Blank Space - Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba = 100 ppm; [Cr, As,Ag,Pb) = 6ppm; [Se, Cd]= 1 ppm; Hg = 0.2 ppm <br />Notes: ''(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (20DOmL). <br />'`EPA S W646 Method 1311, Revision O, July 1992, Section 1.2: If a total analysis of the waste demonstrates that individual acolytes are not present in The waste, <br />or that they ere present but at such low concentrations that the appropriate regulatory levels could not possibly be exceeded, the TCLP need not be run.' <br />Analyst/ Reviewer <br />11