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Key Laboratories, Inc. <br />Client: Walsh Environmental 2479A Riverside Parkway <br />Client Project Name: New Horizon Mine Grand Junction, Colorado 81505-1319 <br />Client Project Number: 900882,0001.010 Phone (970) 243-5311 Fax (970) 243-6010 <br />Client Sample Number: TS-100 <br />Client Sample Location : New Horizon Mine, 0-21 Key Lab .: 10-1010 <br />Sampling Date . 7/15/2010 Work Order 8: 0716101002 <br />Sampling Time: Date Received: 07116110 <br />sample Matrix : Soil Analyst : ,?+ Z'J?? f <br />Sampler: Edward Sample Prep : Total, Open Vessel <br />Analysis Method : "1CP-MS, EPA Malhods 6029/200tlep Method: EPA Method 300.8 Open Vessel Microwave Digrstiaa <br /> Wednesday, <br />Date Analyzed: July 21, 2010 <br />22:03:58 Wednesday, <br />July 21, 2010 <br />19:05:20 <br /> Key Lab Prep Batch Sample !D# M-0720A-10• <br />1010.14 iX10X <br />Sample Comments: <br />Sample Aliquot [mg): 1044.3 <br />Prep Au Spike Recovery: 0.979 <br />Prep/Digestion DF=» 47.88 <br />Pass Audit= » x Total DF=» 478,79 Wi-0720A-10- <br />0000-01 LMS <br />LIMB <br />1000 <br />0.951 <br />s0 <br />5D0.00 <br /> lysis laa mar symbA <br />MrmOa uaaa Rcru. Audit Anal a Reported Value Units <br />tlmlr• Method Blank Blank DF MDL ppm Max OL plant <br />PPm PQL <br /> I «.=# Analytes Reported <br /> ICP-Ma• 7 1m Li Lithium mg/Kg 500.00 025 1 $00 <br /> Ira'-Ma• I+ +o Be Beryllium mgfKg < < < <br /> 10P-'''a• " 10D B Boron mgfKg 500.00 015 2 600 <br /> IcP.Ma• a] ao Na Sodium mglKg < < < <br />IcP-MS• x. 1o Mg Ma nesium mg/Kg < < < <br />Icp.MS• n 1o Al Aluminum mgfKg < < < <br />acv-0.15. zs ,o Si Silicon mgfKg < < < <br />IcP•MS• a1 to P Phosphorus mgfKg < < c <br />IcP-us• s9 ,o K Potassium mgfKg < c < <br />IcP-MS• a as Ca Calcium mgfKg < < e <br />Ira.MS• ae 1o Ti Titanium mgfKg < < < <br />ro0.aE• 5+ 1o V Vanandium mg/Kg < < < <br />IGPMa• ca 10 Cr 100 Chromium mgfKg G < < <br />I-s' as to Mn Man anese tngiXg < < < <br />I--Ma• a. ao Fe Iron mgfKg < < < <br />KP-Ms' 69 to CO Cobalt mgfKg < < c <br />I Ni Nickel mgfKg < <br /> Cn Co er mgfKg < <br /> Zn Zinc mgfKg < <br /> As 100 Arsenic mgfKg 0.48 1,8 1000 <br /> Se 20 x Selenium < mgfKg < 500.00 0.15 1000 <br /> Sr Strontium mgfKg 500.00 0.025 0-1 1000 <br />Ic0.Ma• as fa MD Mol bdenum mg/Kg C < < <br />cr-us 107 m A 100 Silver mg/Kg < c < <br />wrMa• ro + o Cd 20 Cadmium mgtKg < < < <br />ICV-M9' 4] to SLY Antimony mgfKg < < < <br />'G`"a' 1J7 t 0° Ba 2000 Barium mg/Kg 500.00 0,03 0.12 1000 <br />eP a' 802 m Hg 4 Mercury mgfKg c < < <br />x;RNe' ale 10 T) Thallium mgfKg < e < <br />IcP-Ms' mr to Pb 100 Lead mgfKg c < c <br />Icaus• a]x 1W Th Thorium mgfKg 500.00 0.005 0.02 500 <br />IcP-as• aae ,oo U U ranium mg1Kg 500.00 D.005 0.02 50D <br />.Typically, all mantis with >=9olmsl iutc8ration time can be reported. Availableat eustamer4o inquest. <br />Notes: LMB = laboratory method blank, M and MD - sample matrix replicates <br />Notes: LCS = spiked laboratory method blank, MS and MSD - spiked sample matrix replicates <br />Notes: Au is spiked as sample prep surrogate and to facilitate analysts of Mercury, OF = Dilution Factor, <br />Notes: MDL = Method Detection Limit, PQL - PrimaryQuantitatlon Umlk MQL= Maxlmum Ouatditation Limit, <br />Notes: <- less than MDL, J - Greaterthan MDL but less than PQL (4x MDL), E -Estimated Value because it exceeds the MQL <br />Notes: n.a.. Not Applicable, Blank Space - Not Requested or Not Reported <br />Notes: RCRA TCLP Extract Limits: Ba =100 ppm; [Cr, As,A9,Pb) - 5ppm; [Se, Cd) - 1 ppm; Hg = 02 ppm <br />Notes: ''(Total RCRA limits) are 20 times the TCLP extract limits because of TCLP sample size (100g) and extract volume (2000mL). <br />**EPA SW846 Method 1311, Revision 0, July 1992, Section 1.2: "If a total analysis ofthe waste demonstrates that individual analytes are not present in the waste, <br />or that they are present but at suds low concentrations that the appropriate regulatory levels could net possibly be exexded, the TCLP need we be run, ° <br />Analyst / Reviewer <br />