2010-08-18_ENFORCEMENT - C1981008

Home Browse Search

Client: Walsh Environmental ClientPmject Name : New Horizon Mine Client Project Number: 900882.0001.010 Client Sample Number: TS-91 Client Sample Location : New Horizon Mine. 0-18 Sampling Data; 7/1512010 Sampling Time: Sample Mauix: Sail Sampler: Edward Analysis MI:1h d : •ICP-MS, EPA Mittbods 60201200.8 p Method: Key Laboratories, Inc. 2479A Riverside Parkway Grand Junction, Colorado 81505.1319 Phone (970) 243-5311 Fax (970) 243-6010 Ivey tab 9: 10-1002 Work Order r : 0716101002 Data Received: 0711611D 'ry? (I Analyst: V? ,1( t? Sample Prep: Total, Open Vessel r EPA Method 200.8 Open Vessel Microwave Digestion Wednesday, Date Analyzed: July 21, 2010 19:16:59 Wednesday, July 21, 2010 19:28:35 Wednesday, July 21, 2010 19:05:20 Key Lab Prep Batch Sample IDH Wt-0720A-i0. 1002-04_M Sample Comments:, M Sample Aliquot Intgl: 1D71.2 Prep Au Spike Recovery: 0.988 Prep/Digestion DP=>> 46.68 Pass Audit =_» x Total DF=» 466.77 WI-D720A•10. 1002.04_MD MD 1076.3 0.998 46.46 464.55 Wi.0720AA0. 0000-01 LMB LMB 1900 0.951 5o 500.00 analysls loo Tm,• sy,aba RcaA Audit Analyte Reported Value Reported Value Units Meblod Mesa m Lluor" Method Blank Blank DF MDL ppm PQL ppm Max QL ppm 1 cc--#Analytes Reported 1cP•MS' 7 1m Li Lifhlllm mg1K9 600.00 0,25 1 500 ICPMa' 9 1. Be Beryllium mgfKg < < < IcP-MS• 11 nM B Boron mg/Kg 500.00 0.5 2 Soo ILP-Ma' V 1. Na Sodium mgfKg < < < 1w-Mr :4 ,o Mg Magnesium m9 9 < < < IcP•Ma' 27 m Al Aluminum mg/Kg < < < ICP-MS• :e 10 Si Silicon mgfKg < < < anMa' a+ +a P Phosphorus m9lK9 < c < Icp-Ms' a to K Potassium m91Kg < < < ICP•Ms• as to Ca Calcium mgfKg < < < tc P•Ms• as w Ti Titanium mg/Kg < < c IcP-Ms• Si 10 _ V Vanandium mg/Kg < < < ICP-MS• 52 1. Cr 100 Chromium -g/Kg < < < tcP-Ma• ss 1. Mu Manganese mgfKg < < < w 20 Fe Iron mgfKg < < < 1cP-Ma• 59 to Co Cobalt mg/Kg < c < .cP•MS• as to Ni Nickel mg/Kg < < e ICP-Ma- m 1a Cu Copper mg/Kg < < < nPMS- as 10 Zn Zinc mgfKg < < < IcP+us• 7s 1m As 100 Arsenic mgfKg 500.00 0.45 1.B 1000 1c"S• e2 no Se 20 x Selenium 0.16 J < mg/Kg c 500.00 0.15 0.6 1000 ICP-Mr ea 100 St. Strontium mg/Kg 500.00 0.025 0.1 1000 IOP•Ma• 9a 1. Mo Molybdenum mg/Kg < < < ICP-Ma• 107 10 Ag 100 Silver mgfKg < < < ICP-Mr it 10 Cd 20 Cadmium mg/Kg < < < tCAMS' Of 10 Sb Antimony mgfKg < < < lep.- 137 100 Ba 2000 Barium mgfKg 500.00 0.03 0.12 1000 cPMa• 2m to Hg 4 Mercury mgfKg < < < ICP-Mb• 205 10 TI Thallium mg/Kg < < < tcP•MS• 2os 1 Pb 100 Lead mgfKg < < < IcP•MS' n2 too Th Thorium mg/Kg 500.00 D.oos 0.02 Soo IcP-us• 2sa 100 U Uranium mgfKg 500.00 0.005 0.02 Soo -lyptcany, an metals min ?- volmsf imcgralron time can ee repartee. Ayndaate at customers requesr. Notes: LMB =laboratory method blank, M and MO = sample matrix replicates Notes: LCS = spiked laboratory method blank, MS and MSD = spiked sample matrix replicates Notes: Au Is spiked as sample prep surrogate and to facilitate analysis of Mercury, DF - Dilution Factor, Notes: MDL - Method Detection Limit, PQL= Primary Quantitation Limit, MQL= Maximum Quantitation Limit, Notes: < = less than MDL, J = Greater than MDL but less than PQL (4 x MDL), E =Estimated Value because it exceeds the MQL Notes: n.a. = Not Applicable, Blank Space = Not Requested or Not Reported Notes: RCRA TCLP Extract Limits: Ba = 100 ppm; ICr, As,Ag,Pb) - 5ppm; [Se, Cdi = 1 ppm; Hg = 0.2 ppm Notes: "(Total RCRA limits) are 20 timas the TCLP extract limits because of TCLP sample size (100g) and extract volume (2000ml-). -EPA SW846 Method 131 ].Revision 0, July 1997, Section 1.2: "If a total analysis of the waste demonstrates that individual analytes are not present in the waste, or that they are present but at such low concentrations that the appropriate regulatory 1-1t, could not possibly be exceeded, the TCLP need not be run.' Analyst! Reviewer