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Detailed Analytical Report Analytica Environmental Laboratories, Inc. <br />Workorder (SDG): B1005139 <br />Project: M-1977-300 <br />Client: Colorado Division of Reclamation, Mining & Safety <br />Client Project Number: None <br />Report Section: Client Sample Report <br />Client Sample Name: SW-AWD <br />Matrix: Water Collection Date: 5/18/2010 9:45:OOAM <br />Lab Sample Number: B1005139-OIA Analysis Date: 6/4/2010 3:11:19PM <br />Prep Date: 5/26/2010 Instrument: Elan <br />Analytical Method ID: 200.8 - Metals by ICP/MS - Total/TR File Name: 06041 OAsam.c <br />Prep Method ID: 200.8 Dilution Factor: 11 <br />Prep Batch Number: T100527011 <br />Report Basis: As Received Analyst Initials: MMO <br />Sample prep wt./vol: 50.00 ml Prep Extract Vol: 50.00 ml <br />Anal a CASNo Result Flags Units P L MDL run #: <br />Manganese 7439-96-5 47.4 ug/L 0.55 0.19 1 <br />Nickel 7440-02-0 ND ug/L 1.7 0.55 <br />Selenium 778449-2 ND ug/L 5.5 1.5 <br />Silver 7440-22-4 ND ug/L 1.1 0.31 <br />Thallium 7440-28-0 ND ug/L 0.55 0.19 <br />Zinc 7440-66-6 5,25 ug/L 2.8 0.92 <br />The following test was conducted by: Analytica - Thornton <br />Lab Sample Number: B1005139-OIB Analysis Date: 5/21/2010 3:21:48PM <br />Prep Date: 5/21/2010 Instrument: Hach 2500 Col <br />Analytical Method ID: SM4500-PE - Total Phos File Name: <br />Prep Method ID: 4500-PB Dilution Factor: 1 <br />Prep Batch Number: T100521006 <br />Report Basis: As Received Analyst Initials: AT <br />Sample prep wt./vol: 10.00 ml Prep Extract Vol: 10.00 ml <br />Analvte CASNo Result Flags Units P L MDL run #: <br />Phosphorus, Total and Ortho ND mg/L 0.051 0.026 1 <br />The following test was conducted by: Analytica - Thornton <br />Lab Sample Number: B1005139-OIB Analysis Date: 5/24/2010 4:37:47PM <br />Prep Date: 5/24/2010 Instrument: Bubbles K370 <br />Analytical Method ID: SM4500-NH3C - Titrimetric Method - Ammonia, Dist./Titrati File Name: <br />Prep Method ID: 4500-NH313 Dilution Factor: 1 <br />Prep Batch Number: T100524012 <br />Report Basis: As Received Analyst Initials: SM <br />Sample prep wt./vol: 100.00 ml Prep Extract Vol: 100.00 ml <br />Anal a CASNo Result Flags Units POLL MDL run <br />Ammonia as N 7664-41-7 1.8 mg/L 0.40 0.11 1 <br />The following test was conducted by: Analytica - Thornton <br />Page 5 of 75