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Detailed Analytical Report Analytica Environmental Laboratories, Inc. <br />Workorder (SDG): B1005139 <br />Project: M-1977-300 <br />Client: Colorado Division of Reclamation, Mining & Safety <br />Client Project Number : None <br />Report Section: Method Blank Report <br />Client Sample Name: MB <br />Matrix: Aqueous Collection Date: 6/1/2010 5:00:OOPM <br />Lab Sample Number: T100601019-MB Analysis Date: 6/1/2010 5:15:OOPM <br />Prep Date: 6/1/2010 Instrument: Bubbles K370 <br />Analytical Method ID: SM4500-NH3C - Titrimetric Method - Ammonia, Dist./Titrati File Name: <br />Prep Method ID: 4500-NH3B Dilution Factor: 1 <br />Prep Batch Number: T100601019 <br />Report Basis: As Received Analyst Initials: AT/SM <br />Sample prep wt./vol: 100.00 ml Prep Extract Vol: 100.00 ml <br />Anal a CASNo Result Flags Units IQ MDL run <br />Ammonia as N 7664-41-7 ND mg/L 0.40 0.11 1 <br />The following test was conducted by: Analytica - Thornton <br />Lab Sample Number: T100525018-MB Analysis Date: 5/25/2010 10:00:00AM <br />Prep Date: 5/24/2010 Instrument: Hach 2500 Col <br />Analytical Method ID: SM4500-CNE - Cyanide, Colorimetric Method - Total CN File Name: <br />Prep Method ID: 4500-CNB Dilution Factor: 1 <br />Prep Batch Number: T100525018 <br />Report Basis: As Received Analyst Initials: SCM/AT <br />Sample prep wt./vol: 500.00 ml Prep Extract Vol: 100.00 ml <br />Anal a CASNo Result Flags Units P L MDL run <br />Cyanide ND mg/L 0.0040 0.0021 1 <br />The following test was conducted by: Analytica - Thornton <br />Lab Sample Number: T100521002-MB Analysis Date: 5/20/2010 5:35:47PM <br />Prep Date: 5/20/2010 Instrument: IC <br />Analytical Method ID: Inorganic Anions by Ion Chromatography - Nitrate&Nitrite by IC File Name: 100520_008.1) <br />Prep Method ID: 300.0 Dilution Factor: 1 <br />Prep Batch Number: T100521002 <br />Report Basis: As Received Analyst Initials: C S <br />Sample prep wt./vol: 20.00 ml Prep Extract Vol: 20.00 ml <br />Anal a CASNo Result Flags Units P L MDL run #: <br />Total Nitrate & Nitrite as N ND mg/L 0.80 0.039 1 <br />The following test was conducted by: Analytica - Thornton <br />Lab Sample Number: T100524007-MB Analysis Date: 5/21/2010 2:26:46PM <br />Prep Date: 5/21/2010 Instrument: IC <br />Analytical Method ID: Inorganic Anions by Ion Chromatography - Anions by IC File Name: 100521_008.1) <br />Prep Method ID: 300.0 Dilution Factor: 1 <br />Prep Batch Number: T100524007 <br />Report Basis: As Received Analyst Initials: C S <br />Sample prep wt./vol: 20.00 ml Prep Extract Vol: 20.00 ml <br />Anal a CASNo Result Flags Units IQ MDL run #: <br />Chloride ND mg/L 0.80 0.042 1 <br />Fluoride ND mg/L 0.40 0.031 <br />Page 52 of 75