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Detailed Analytical Report Analytica Environmental Laboratories, Inc. <br />Workorder (SDG): B1005139 <br />Project: M-1977-300 <br />Client: Colorado Division of Reclamation, Mi ning & Safety <br />Client Project Number : None <br />Report Section: Client Sample Report <br />Client Sample Name: SW-BPL <br />Matrix: Water Collection Date: 5/18/2010 2:00:OOPM <br />Lab Sample Number: B1005139-04A Analysis Date: 6/4/2010 3:58:46PM <br />Prep Date: 5/26/2010 Instrument: Elan <br />Analytical Method ID: 200.8 - Metals by ICP/MS - Total/TR File Name: 060410Asam.c <br />Prep Method ID: 200.8 Dilution Factor: 11 <br />Prep Batch Number: T100527011 <br />Report Basis: As Received Analyst Initials: MMO <br />Sample prep wt./vol: 50.00 ml Prep Extract Vol: 50.00 ml <br />Anal a CASNo Result Flags Units PQL MDL run #: <br />Manganese 7439-96-5 44.3 ug/L. 0.55 0.19 1 <br />Nickel 7440-02-0 1.70 ug/L 1.7 0.55 <br />Selenium 7784-49-2 ND ug/L 5.5 1.5 <br />Silver 7440-22-4 ND ug/L 1.1 0.31 <br />Thallium 7440-28-0 ND ug/L 0.55 0.19 <br />Zinc 7440-66-6 5.15 ug/L 2.8 0.92 <br />The following test was conducted by: Analytica - Thornton <br />Lab Sample Number: B1005139-04B Analysis Date: 5/21/2010 3:21:48PM <br />Prep Date: 5/2112010 Instrument: Hach 2500 Col <br />Analytical Method ID: SM4500-PE - Total Phos File Name: <br />Prep Method ID: 4500-PB Dilution Factor: I <br />Prep Batch Number: T100521006 <br />Report Basis: As Received Analyst Initials: AT <br />Sample prep wt./vol: 10.00 ml Prep Extract Vol: 10.00 ml <br />Anal a CASNo Result Flaps Units Q MDL run #: <br />Phosphorus, Total and Ortho 0.094 mg/L 0.051 0.026 1 <br />The following test was conducted by: Analytica - Thornton <br />Lab Sample Number: B1005139-04B Analysis Date: 5/24/2010 4:37:47PM <br />Prep Date: 5/24/2010 Instrument: Bubbles K370 <br />Analytical Method ID: SM4500-NH3C - Titrimetric Method - Ammonia, Di st./Titrati File Name: <br />Prep Method ID: 4500-NH3B Dilution Factor: 1 <br />Prep Batch Number: T100524012 <br />Report Basis: As Received Analyst Initials: SM <br />Sample prep wt./vol: 100.00 ml Prep Extract Vol: 100.00 ml <br />Anal a CASNo Result Flags Units P L MDL <br />Ammonia as N 7664-41-7 ND mg/L 0.40 0.11 <br />run #: <br />1 <br />The following test was conducted by: Analytica - Thornton <br />Page 14 of 75