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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY <br />Login Number: D12928 <br />Account: NUVECOB - Nuvemco, LLC <br />Project: Last Chance <br />QC Batch ID: MP1883 Methods: SW846 6020 <br />Matrix Type: AQUEOUS Units: mg/l <br />Prep Date: 05/14/10 <br />D12928-1 Spikelot MSD QC <br />Metal Original MSD MPICPALL % Rec RPD Limit <br />Aluminum <br />Antimony 0.0015 1.0 1.0 99.8 0.0 <br />Arsenic 0.0015 0.99 1.0 98.9 1.0 <br />Barium <br />Beryllium 0.0 0.52 0.50 104.0 3.9 <br />Boron <br />Cadmium 0.0 0.49 0.50 98.0 2.1 <br />Calcium <br />Chromium <br />Cobalt <br />Copper <br />Iron <br />Lead <br />Magnesium <br />Manganese <br />Molybdenum <br />Nickel <br />Phosphorus <br />Potassium <br />Selenium <br />Silver <br />Sodium <br />Strontium <br />Thallium 0.0 0.99 1.0 99.0 3.1 <br />Tin <br />Titanium <br />Uranium 0.0020 1.0 1.0 99.8 0.0 <br />Vanadium <br />Zinc <br />Associated samples MP1883: D12928-1, D12928-2, D12928-3 <br />Results < IDL are shown as zero for calculation purposes <br />(*) Outside of QC limits <br />(N) Matrix Spike Rec. outside of QC limits <br />(anr) Analyte not requested <br />20 <br />20 <br />20 <br />20 <br />20 <br />20 <br />Page 2 <br />LTI <br />W <br />N <br />® 32 of 33 <br />EACCUTEST. <br />D12928 Laboratories