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~~~ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Kerr Coal Company ACZ Project ID: L56030 <br />~f i .. <br />L56070-0t WG204874 Chlodtle M325.2 - Colodmetric RA Relative Percent Difference (RPD) was not used far data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />WG20474fi NitratelNitrite as N, dissolvetl M353.2 -AUtomatetl Catlmium RA Relative Percent Difference (RPD) was not used for tlata <br /> Reduction validation because the sample concentration is too low for <br /> acwrate evaluation (< 10x MDL). <br /> Nitrite as N, dissolved M353.2 -Automated Cadmium R4 Relatve Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low far <br /> accurate evaluatlon (< IDx MDL). <br />WG204928 Sulfate SM6500 S04-D RA Relative Percent Difference (RPD) was not used for tlata <br /> valitlalion because the sample concentration is too low for <br /> acwrate evaluation (< 10x MDL). <br />L56030-02 WG204874 Chloride M325.2 - Colodmetric RA Relative Percent Difffference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> acwrate evaluation (< 10x MDL). <br />WG204746 Nitrate/Nitrite as N, dissolved M353.2 -Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />Nitrite as N, tlissalved M353.2 -Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Retluction validation because the sample concentration is too low for <br /> acwrate evaluation (< tOx MDL). <br />WG204928 Sulfate SM4500 504D Pot Relative Percent Difference (RPD) was not used for tlata <br /> validation because the sample concentration is too low far <br /> accurate evaluation (< 10x MDL). <br />L56030.03 WG204874 Choride M325.2 - Colodmetr!c RA Relative Percent Difference (RPD) was not used for data <br /> valitlalion because the sample concentration is too low for <br /> accurate evaluation (< tOx MDLj. <br />WG204746 Nitrate/Nitrite as N, dissolved M353.2 -Automatetl Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> acwrate evaluation (< 10x MDL). <br />NiMte as N, dissolved M353.2 - Automatetl Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< tOx MDL). <br />WG204928 Sulfate SM4500 S04-D RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluatlon (< 10x MDL). <br />L56030-04 WG205008 Sodium, dissolved M200.7 ICP D2 Sample required dilution. Target analyte exceeded <br /> calibration range. <br />WG204874 Chloride M325.2 - Colorimetric RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> acwrate evaluatlon (< 10x MOL). <br />WG204746 Nitrate/Nitrite as N, dissolved M353.2 -Automated Cadmium R4 Relative Percent D'rfrerence (RPD) was not used for data <br /> Reduction validation bepuse the sample mncenhation is too low far <br /> accurate evaluation (< tOx MDL). <br />NiMte as N, dissolved M353.2 -Automated Cadmium RA Relatve Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample wncentration is too low for <br /> acwrate evaluation (< 10x MDL). <br />WG204915 Residue. Filterable (TDS) @180C M160.1 - Gravimetnc ZO TDS concentration is based on a final resitlue greater than <br /> 200 mg. <br />WG204926 Sulfate SM4500 504-D RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> acwate evaluatlon (< 10x MDL). <br />L56030-05 WG205008 Sodium, dissolved M200.71CP D2 Sample required dilution. Target analyle exceeded <br /> calibration range. <br />WG204746 Nitrate/Nitrite as N, dissolved M353.2 -Automated Cadmium RA Relative Percent Difference (RPD) was no[ used for data <br /> Retluction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />NiMte as N, dissolved M353.2 -Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample wncentmtlon is too low for <br /> acwrate evaluation (< 10x MDL). <br />WG204928 Sulfate SM4500 S04-D R4 Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too law for <br /> acwrate evaluation (< 10x MOL). <br />REPAD.15.06.05.01 <br />L56030: Page 12 of 19 <br />