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ADZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Sorinos. CO 80487 !8001 334-A4A3 <br />Metals Analysis <br />Calcium, dissolved M200.7 ICP 110 mg/L 0.2 1 06/11/08 1:07 aeh <br />Iron, dissolved M200.7 ICP U mg/L 0.02 0.05 06/11/08 1:07 aeh <br />Magnesium, dissolved M200.7 ICP 29.8 mg/L 0.2 1 06/11/08 1:07 aeh <br />Manganese, dissolved M200.7 ICP U mg/L 0.005 0.03 06/11/08 1:07 aeh <br />Selenium, total <br />recoverable SM 3114 B, AA-Hydride _ U mg/L 0.001 0.005 06/10/08 14:47 pmc <br />Sodium, dissolved M200.7 ICP - 137 mg/L 0.3 2 06/11/08 1:07 aeh <br />Wet Chemistry <br /> <br />Alkalinity as CaC03 SM2320B - Titration <br />Bicarbonate as 289 mg/L 2 20 06/09/08 0:00 jif <br />CaC03 <br />Carbonate as CaC03 14 B mg/L 2 20 06/09/08 0:00 jif <br />Hydroxide as CaC03 U mg/L 2 20 06/09/08 0:00 jif <br />Total Alkalinity 303 mg/L 2 20 06/09/08 0:00 jif <br />Chloride - SM45000I-E 20 mg/L 1 5 06/10/0810:53 aml <br />Lab Filtration SM 3030 B 06/02/08 15:39 Izg <br />Lab Filtration & SM 3030 B 06/02/08 14:00 Izg <br />Acidification <br />Nitrate as N, dissolved Calculation: N03NO2 minus N02 0.44 mg/L 0.02 0.1 06/26/08 13:25 talc <br />Nitrate/Nitrite as N, M353.2 - Automated Cadmium 0.44 H * mg/L 0.02 0.1 06/03/08 22:10 pjb <br />dissolved Reduction <br />Nitrite as N, dissolved M353.2 - Automated Cadmium UH * mg/L 0.01 0.05 06/03/08 22:10 pjb <br /> Reduction <br />Phosphate Calculation based on Ortho 0.09 B mg/L 0.03 0.15 06/26/08 13:25 calc <br /> Phosphorus <br />Phosphorus, ortho M365.1 - Automated Ascorbic 0.03 BH * mg/L 0.01 0.05 06/03/08 20:53 pjb <br />dissolved Acid <br />Residue, Filterable SM2540C 870 mg/L 10 20 06/04/08 11:40 gkj <br />(TDS) @180C <br />Residue, Non- SM2540D 9 B * mg/L 5 20 06104/08 10:33 jif <br />Filterable (TSS) <br />@105C <br />Sodium Absorption USGS - 11738-78 3.02 0.03 0.15 06/26/08 13:25 talc <br />Ratio in Water <br />Sulfate 375.4 - Turbidimetric 320 mg/L 10 50 06/19/08 15:24 ccp <br />REPIN.02.06.05.01 <br />* Please refer to Qualifier Reports for details. <br />Page 3 of 11 <br />Energy Fuels Coal, Inc. (Southfield) ACZ Sample ID: L69590-01 <br />Project ID: SOUTHFIELD Date Sampled: 05128108 14:52 <br />Sample ID: LOWER OAK CRK Date Received: 06102108 <br />Sample Matrix: Surface Water