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1 <br />ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />Kerr Coal Company ACZ Project ID: L69087 <br />ACZID .WORKNUM PARAMETER .D <br /> <br />L69087-06 WG244576 Chloride 325.2 / SM45000I-E RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< IN MDL). <br />WG244156 Nitrate/Nitrite as N, dissolved M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation.(- 10x MDL). <br />Nitrite as N, dissolved M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br /> Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />WG244533 Sulfate SM4500 S04-D RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />L69087-07 WG244576 Chloride <br />WG244156 Nitrate/Nitrite as N, dissolved <br />Nitrite as N, dissolved <br />WG244343 Residue. Filterable (TDS) @180C <br />WG244533 Sulfate <br />325.21 SM45000I-E RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br />Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />M353.2 - Automated Cadmium RA Relative Percent Difference (RPD) was not used for data <br />Reduction validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />160.1 / SM2540C RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />SM4500 S04-D RA Relative Percent Difference (RPD) was not used for data <br /> validation because the sample concentration is too low for <br /> accurate evaluation (< 10x MDL). <br />REPAD.15.06.05.01 <br />Page 10 of 16