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047 <br />Evergreen Analytical, Inc. <br />Rork Order: 08-4900 <br />Client Project ID: <br />Date: 16-Jul-08 <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: R40590 <br />Sample ID: Blank SampType: MBLK TestCode: 1664_W Run ID: FTIR 0807118 Prep Date: 7/1112008 Units: mg/L <br />Batch ID: R40690 TestNo: El 664A FileID: 1 Analysis Date: 7/1112008 SegNo: 712654 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />HEM - Oil & Grease U 5.00 <br />Sample ID: LCS SampType: LCS TestCode: 1664_W Run ID: FTIR_080711B Prep Date: 7/1112008 Units: mg/L <br />Batch ID: R40590 TestNo: Ell 664A FileID: 2 Analysis Date: 7/1112008 SegNo: 712655 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />HEM - 011 & Grease 39.6 5.00 40 0 99 70 130 0 0 <br />Sample ID: LCSD SampType: LCSD TestCode:1664_W Run ID: FTIR 080711B Prep Date: 711112008 Units: mg/L <br /> Batch ID: R40590 TestNo: E1664A FileID: 3 Analysis Date: 7/1112008 SegNo: 712656 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />HEM - Oil & Grease 41 5.00 40 0 103 70 130 39.6 3.47 30 <br />Sample ID: 08-4637-16AMS SampType: MS TestCode: 1664_W Run ID: FTIR_080711B Prep Date: 7/1112008 Units: mg/L <br />Batch ID: R40590 TestNo: E1664A FileID: 8 Analysis Date: 711112008 SegNo: 712661 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowi-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />HEM - Oil & Grease 39.2 5.00 40 25.9 33.3 70 130 0 0 t <br />Qualifiers: U - Not detected at or above the Reporting Limit R- RPD outside acceptance limits <br />J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br />S - Spike Recovery outside acceptance limits H - Prep or analytical holding time exceeded <br />E - Extrapolated value, value exceeds calibration range. X - See case narrative <br />i i -11 is _ _ _ _ ? _ _ _ _ _ _ _ _ M