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043 <br />Evergreen Analytical, Inc. <br />Work Order: 08-4900 <br />Client Project ID: <br />Date: 23-Jul-08 <br />ANALYTICAL QC SUMMARY REPORT <br />Batch[D: 16047 <br />Sample ID: MB-16047 SampType: MBLK TestCode: 200.8_D Run ID: ICPMS_080714A Prep Date: 7/14/2008 Units: mg/L <br /> Batch ID: 16047 TestNo: E200.8 FileID: 080714A.B\048SMPL.D Analysis Date: 7114/2008 SegNo: 711777 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] <br />Antimony U 0.00200 <br />Arsenic U 0.00200 <br />Cadmium U 0.000500 <br />Copper U 0.0100 <br />Lead U 0.00100 <br />Selenium U 0.00200 <br />Silver U 0.000200 <br />Thallium U 0.00100 <br />Sample ID: LCS-16047 SampType: LCS TestCode: 2D0.8_D Run ID: ICPMS_080714A Prep Date: 7/14/2008 Units: mg/L <br /> Batch ID: 16047 TestNo: E200.8 FileID: 080714A.B\054SMPL.D Analysis Date: 7114/2008 SegNo: 711781 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Antimony 0.02507 0.00200 0.025 0 100 85 115 0 0 <br />Arsenic 0.2526 0.00200 0.25 0 101 85 115 0 0 <br />Cadmium 0.02517 0.000500 0.025 0 101 85 115 0 0 <br />Copper 0.2506 0.0100 0.25 0.001145 100 85 115 0 0 <br />Lead 0.0486 O.D0100 0.05 0 97.2 85 115 0 0 <br />Selenium 0.0553 0.00200 0.05 0 111 85 115 0 0 <br />Silver 0.0249 0.000200 0.025 0 99.6 85 115 0 0 <br />Thallium 0.01259 0.00100 0.0125 0 101 85 115 0 0 <br />Sample ID: 08-4900-01FMS SampType: MS TestCode: 200.813 Run ID: ICPM5 080714A Prep Date: 7/14/2008 Units: mg/L <br />Client ID: MW-02 Batch ID: 18047 TestNo: E200.8 FileID: 080714A.B\057SMPL.D Analysis Date: 7/14/2008 SegNo: 711783 <br />Analyte Result LQL SPKvalue SPK Ref Val . %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Antimony 0.024 0.00200 0.025 0.0001273 96 70 130 0 0 <br />Arsenic 0.2646 0.00200 0.25 0.0008655 106 70 130 0 0 <br />Cadmium 0.02383 0.000500 0.025 0 95.3 70 130 0 0 <br />Qualifiers: U - Not detected at or above the Reporting f .imit R - RPD outside acceptance limits <br /> J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br /> S - Spike Recovery outside acceptance limits H - Prep or analytical holding time exceeded <br /> E - Extrapolated value, value exceeds calibration range. X - See case narrative <br />