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040 <br />Work Order: 08-4900 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 16089 <br />Sample ID: LCS-16089 SampType: LCS TestCode: 200.71) Run ID: ICP-OPTIMA 5300 DV_080717A Prep Date: 7/17/2008 Units: mg/L <br /> Batch ID: 16089 TestNo: E200.7, Rev. FileID: 07170813M Analysis Date: 7117/2008 SegNo: 713896 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC LDWLImlt HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Beryllium 0.04606 0.000450 0.05 0 92.1 75.1 114 0 0 <br />Boron 1.89 0.0200 2 0 94.5 79 125 0 0 <br />Calcium 9.592 0.387 10 0 95.9 74 113 0 0 <br />Chromium 1.813 0.0100 2 0 90.7 76.2 115 0 0 <br />Cobalt 1,765 0.00500 2 0 88.2 72.1 110 0 0 <br />Iron 4.778 0.0700 5 0 95.6 76.6 115 0 0 <br />Magnesium 9.544 0.150 10 0 95.4 76.7 114 0 0 <br />Manganese 1.781 0.00500 2 0 89 72.4 109 0 0 <br />Nickel 1.747 0.0300 2 0 B7.3 69.9 115 0 0 <br />Potassium 10.25 0.340 10 0.09716 102 70.9 115 0 0 <br />Silver 0.1959 0.0300 0.2 0 98 61 112 0 0 <br />Sodium 9.834 0,400 10 0 98.3 80 120 0 0 <br />Vanadium 1.845 0.0100 2 0 92.2 76.4 112 0 0 <br />Zinc 1.799 0.0300 2 0 90 68.5 112 0 0 <br />Silicon as Si02(Silica) 10.55 0.107 10.65 0 99.1 77.3 115 0 0 <br />Sample ID: LCS-16089 SampType: LCS TestCode: 2D0.7_D Run ID: ICP-OPTIMA 5300 DV_080723A Prep Date: 7117/2008 Units: mg/L <br /> Batch ID: 16089 TestNo: E200.7, Rev. FileID: 07220OLISR Analysis Date: 7/23/2008 SegNo: 716107 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ <br />Lithium 1.93 0.00200 2 0 96.5 75 125 0 0 <br />Sample ID: 084900-01FMS SampType: MS TestCode: 200.713 Run ID: ICP-OPTIMA 5300 DV_080717A Prep Date: 7/1712008 Units: mg/L <br />Client ID: MW-02 Batch ID: 16089 TestNo: E200.7, Rev. FileID: 071708113M Analysis Date: 7/1712008 SegNo: 713898 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Aluminum 2.524 0.125 2.5 0.01745 101 75 125 0 0 <br />Barium 5.812 0.00250 6.25 0.03017 92.5 75 125 0 0 <br />Beryllium 0.05583 0.000563 0.0625 0 89.3 75 125 0 0 <br />Boron 2.439 0.0250 2.5 0.09856 93.6 75 125 0 0 <br /> <br />Qualifiers: U - Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br /> J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br /> S - Spike Recovery outside acceptance limits H - Prep or analytical holding time exceeded <br /> E - )extrapolated value, value exceeds calibratiar range. X - See case narrative <br />0= = M M M M M = M M r M M = M M M