PERMIT FILE - 9/3/2008, 9:13:34 AM-MR1

• Permit No: P2008043
• IBM Index Class Name: PERMIT FILE
• Doc Date: 8/12/2008
• Doc Name: Needed items for NOI
• From: Powertech ‎(USA)‎ Inc.
• To: DRMS
• Email Name: ACS
• Media Type: D
• Archive: No

SOP No. 11.0 Sample Management
Table 1
CHEMICAL ANALYSES
Estimated
Number of LAB
QC Sam pies b Estimated Number of FIELD QC Sam pies Number of
Analytical MSD Container(s))
Method Sample or Trip Field Rinsate Minimum Volume Sample Hold Time
Analytical Parameter (a) Matrix MS DUP Field Du Blank Blank Blank c Preservation (d) (from collection)
Total Metals except SW-846 Water 1 per 20 1 per 20 NA 0 1 per 20 pH < 2 with HN03 I I -liter poly 180 days
Mercury 6020/601OB samples samples samples
Total Metals except SW-846 Sed/soil 1 per 20 1 per 20 NA 0 I per 20 Cool to 4 °C 116-oz poly or glass 180 days
Mercury 6020/601OB samples samples samples
Total Metals except SW-846 Biota 1 per 20 See SOP (e) NA 0 l per 20 On ice See SOP (e) 180 days
Mercury 6020/601 OB samples samples
Total Mercury SW-846 7470A Water 1 per 20 1 per 20 NA 0 1 per 20 pH < 2 with HN03 1 500-m1 poly 28 days
samples samples samples
Total Mercury SW-846 Sed/soil I per 20 1 per 20 NA 0 1 per 20 Cool to 4 °C 116-oz poly or glass 28 days
7471A samples samples samples
Total Mercury SW-846 7471 A Biota 1 per 20 See SOP (e) NA 0 1 per 20 On ice See SOP (e) 28 days
samples samples
Diss. Metals except SW-846 Water 1 per 20 1 per 20 NA 0 1 per 20 pH < 2 with HN03 1 I-liter poly 180 days
Mercury 6020/601OB samples samples samples
Diss. Mercury SW-846 7470A Water 1 per 20 1 per 20 NA 0 1 per 20 pH < 2 with HN03 1 500-m1 poly 28 days
samples samples samples
Anions SW-846 0056 or Water 1 per 20 1 per 20 NA 0 1 per 20 Cool to 4°C 1 250-m1 poly 28 days
(Sulfate, Chloride) EPA 300.0 samples samples samples
Anions SW-846 0056 or Sed/soil I per 20 1 per 20 NA 0 1 per 20 Cool to 4°C 1 16-oz glass 28 days
(Sulfate, Chloride) EPA 300.0 samples samples samples
Fluoride 340.2 Water I per 20 l per 20 NA 0 1 per 20 Cool to 4°C 1 - 250 ml poly 28 days
samples samples samples
Fluoride 340.2 Sediment 1 per 20 1 per 20 NA 0 1 per 20 Cool to 4°C l - 16 oz glass 28 days
samples samples samples
Ammonia as N EPA 350.1 Water 1 per 20 1 per 20 NA 0 1 per 20 pH < 2 H2SO4 1- 500 ml poly 28 days
samples samples samples
Nitrate/Nitrite as N EPA 353.1 Water 1 per 20 1 per 20 NA 0 I per 20 pH < 2 H2SO4 1- 250 ml poly 28 days
samples samples samples
Nitrite as N EPA 354.1 Water 1 per 20 1 per 20 NA 0 1 per 20 Cool to 4°C I - 250 ml poly 48 hours
samples samples samples
Hexavalent Chromium SW-846 7106A Water 1 per 20 1 per 20 NA 0 1 per 20 Cool to 4°C I - 250 ml poly 24 hours
samples samples samples
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