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939 Evergreen Analytical, Inc. <br />Work Order: 08-2533 <br />Client Project ID: <br />Date: 22-Apr-08 <br />ANALYTICAL QC SUMMARY RE, PORT <br />TestCode: ALK WGRP <br />Sample ID MBLK SampType: MBLK TestCode: ALK_WGRP Run ID: ALK_080416B Prep Date: 4116/2008 Units: mg/L CaC03 <br /> Batch ID: R38487 TestNo: SM2320B FileID: 72 Analysis Date: 4/16/2008 SegNo: 677076 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Total Alkalinity U 5.0 <br />Sample ID LCS SampType: LCS TestCode: ALK_WGRP Run ID: ALK_080416B Prep Date: 4/16/2008 Units: mg/L CaCO3 <br />Batch ID: R38487 TestNo: SM2320B FileID: 73 Analysis Date: 4/16/2008 SegNo: 677077 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowlimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />:al Alkalinity <br />99.25 5.0 100 0 99.2 90 110 0 0 <br />Qualifiers: U - Not detected at or above the Reporting Limit R - RPD outside acceptance limits <br />J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br />S - Spike Recovery outside acceptance limits Il - Prep or analytical holding time exceeded <br />E - Extrapolated value, value exceeds calibration range. X - See case narrative