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GZS <br />Work Order: 08-2533 <br />Client Project ID: <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 15253 <br />Sample ID: LCS-15253 SampType: LCS TestCode: 200.713 Run ID: ICP-OPTIMA 5300 OV_080417A Prep Date: 4117/2008 Units: mg/L <br /> Batch ID: 15253 TestNo: E200.7, Rev. FileID: 041708PM Analysis Date: 4/17/2008 SegNo: 677746 <br />Analyte Result LQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Barium 5.207 0.00200 5 0 104 80.1 112 0 0 <br />Beryllium 0.05132 0.000450 0.05 0 103 75.1 114 0 0 <br />Boron 2.07 0.0200 2 0 103 79 125 0 0 <br />Calcium 10.46 0.387 10 0 105 74 113 0 0 <br />Chromium 1.99 0.0100 2 0 99.5 76.2 115 0 0 <br />Cobalt 1.959 0.00500 2 0 97.9 72.1 110 0 0 <br />Iron 5.285 0.0700 5 0 106 76.6 115 0 0 <br />Magnesium 10.6 0.150 10 0 106 76.7 114 0 0 <br />Manganese 1.95 0.00500 2 0 97.5 72.4 109 0 0 <br />Nickel 1.966 0.0300 2 0 98.3 69.9 115 0 0 <br />Potassium 10.54 0.340 10 0 105 70.9 115 0 0 <br />Silver 0.1804 0.0300 0.2 0 90.2 61 112 0 0 <br />Sodium 10.69 0.400 10 0 107 80 120 0 0 <br />Vanadium 1.994 0.0100 2 0 99.7 76.4 112 0 0 <br />Zinc 2.015 0.0300 2 0 101 68.5 112 0 0 <br />Silicon as Si02(Silica) 11.36 0.107 10.65 0 107 77.3 115 0 0 <br />Sample ID: LCS-15253 SampType: LCS TestCode: 200.7D Run ID: ICP-OPTIMA 5300 DV_0804258 Prep Date: 4/17/2008 Units: mg/L <br /> Batch ID: 15253 TestNo: E200.7, Rev. FileID: 042508PM Analysis Date: 4/25/2008 SegNo: 680953 <br />Analyte Result LQL SPKvalue SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Lithium 2.059 0.00200 2 0 103 75 125 0 0 <br />QuefiSers: U - Not detected at or above the Reporting Limit <br />J - Analytc detectcd bclow quantitation limits <br />S - Spike Recovery outside acceptance limits <br />E - Extrapolated value, value exceeds calibration range. <br />R - RPD outside acceptance limits <br />B - Analyte detected in the associated Method Blank <br />H - Prep or analytical holding time exceeded <br />X - See case narrative <br />? ,M = M r r mm ? r = M m m m r m m M