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ACIZ Laboratories, Inc. _ - <br />2773 Downhill Drive Steamboat Springs, CO 80487(800) 334-5493 L <br />I <br />Kerr Coal Company ACZ Sample ID: L62082-03 <br />Project ID: Date Sampled: 04118107 11:30 <br />Sample ID: 79-1 Date Received: 04118107 <br /> Sample Matrix: Ground Water <br />Metals Analysis <br /> <br /> <br />Calcium, dissolved M200.7 ICP 13.2 mg/L 0.2 1 04/24/07 21:00 1 djt <br />Iron, dissolved M200.7 ICP 0.12 mg/L 0.02 0.05 04/25/07 17:51 djt <br />Magnesium, dissolved M200.7 ICP 1.0 mg/L 0.2 1 04/24/07 21:00 djt <br />Manganese, dissolved M200.7 ICP 0.038 mg/L 0.005 0.0 3 04124/07 21:00 djt <br />Potassium, dissolved M200.7 ICP 1.6 B mg/L 0.3 2 04/24/07 21:00 djt <br />Sodium, dissolved M200.7 ICP 413 mg/L 0.3 2 04124/07 21:00 I djt <br />Wet Chemistry <br />Alkalinity as CaC03 SM2320B - Titration <br />Bicarbonate as <br />CaC03 <br />Carbonate as CaC03 <br />Hydroxide as CaC03 <br />Total Alkalinity <br />Cation-Anion Balance Calculation <br />Cation-Anion Balance <br />Sum of Anions <br />Sum of Cations <br />Chloride M325.2 - Colorimetric <br />Hardness as CaC03 SM2340B - Calculation <br />Lab Filtration SM 3030 B <br />Lab Filtration & SM 3030 B <br />Acidification <br />Nitrate as N, dissolved Calculation: N03NO2 minus N02 <br />Nitrate/Nitrite as N, M353.2 - Automated Cadmium <br />dissolved Reduction <br />Nitrite as N, dissolved M353.2 - Automated Cadmium <br /> Reduction <br />Residue, Filterable M160.1 - Gravimetric <br />(TDS) @180C <br />Sodium Absorption USGS - 11738-78. <br />Ratio in Water <br />Sulfate SM4500 S04-D. <br />TDS (calculated) Calculation <br />TDS (ratio - Calculation <br />measured/calculated) <br />673 <br />21 <br />U <br />694 <br />-5.5 <br />21.2 <br />19.0 <br />260 <br />37 <br />1190 <br />29.80 <br />1110 <br />1.07 <br />mg/L 2 20 04/24/07 0:00 <br />mg/L 2 20 04/24/07 0:00 <br />mg/L 2 20 04/24/07 0:00 <br />mg/L 2 20 04/24/07 0:00 <br />cas <br />cas <br />cas <br />cas <br /> % 04/27/07 0:00 calc <br /> meq/L 0.1 0.5 04/27/07 0:00 calc <br /> meq/L 0.1 0.5 04/27/07 0:00 calc <br /> mg/L 10 50 04/24/0713:50 jag <br /> mg/L 1 7 04/27/07 0:00 calc <br />* 04/19/0710:34 mis <br />* 04/19/0711:58 mis <br />U mg/L 0.02 0.1 04/27/07 0:00 calc <br />U * . mg/L 0.02 0.1 04/18/07 21:54 pjb <br />U mg/L 0.01 0.05 04/18/07 21:54 pjb <br /> mg/L 10 20 04/19/0714:58 seb <br /> 0.03 0.15 04/27/07 0:00 calc <br />U mg/L 10 50 04/23/07 9:21 aeh/wpa <br /> mg/L 10 50 04/27/07 0:00 calc <br /> 04/27/07 0:00 calc <br />REPIN.02.06.05.01 * Please refer to Qualifier Reports for detail. <br />I <br />L62082: Page 5 of 17