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<br />LABORATORY CONTROL SAMPLE DATA REPORT
<br />Trace Level Organic Compounds
<br />Client Lot #---: D2L050322 Work Order #--.= FEMV7IAC
<br />LCS Lot-Sample#: G2L110000-510
<br />Prep Date...._.: 12/11/02 Analysis Date..: 12/14/02
<br />Prep Batch #---: 2345510 Analysis Time..: 12:22
<br />Dilution Factor: 1
<br />PARAMETEP,
<br />2,3,7,8-TCDD
<br />1,2,3,7,8-PeCDD
<br />1,2,3,4,7,8-HxCDD
<br />1,2,3,6,7,8-HxCDD
<br />1,2,3,7,8,9-HxCDD
<br />1,2,3,4,6,7,8-HpCDD
<br />OCDD
<br />2,3,7,8-TCDF
<br />1,2,3,7,8-PeCDF
<br />2,3,4,7,8-PeCDF
<br />1,2,3,4,7,8-HxCDF
<br />1,2,3,6,7,8-HxCDF
<br />2,3,4,6,7,8-HxCDF
<br />1,2,3,7,8,9-HxCDF
<br />1,2,3,4,6,7,8-HpCDF
<br />1,2,3,4,7,8,9-HpCDF
<br />OCDF
<br />SPIKE
<br />100
<br />100
<br />100
<br />100
<br />100
<br />200
<br />20.0
<br />100
<br />100
<br />100
<br />100
<br />100
<br />100
<br />100
<br />100
<br />200
<br />MEASURED
<br />AMOUNT
<br />18.7
<br />101
<br />103
<br />101
<br />103
<br />101
<br />206
<br />19.2
<br />98.2
<br />106
<br />95.7
<br />93.2
<br />107
<br />99.5
<br />99.9
<br />96.0
<br />186
<br />INTERNAL STANDARD
<br />13C-2,3,7,8-TCDD
<br />13C-1,2,3,7,8-PeCDD
<br />13C-1,2,3,6,7,8-HxCDD
<br />13C-1,2,3,4,6,7,8-HpCDD
<br />13C-OCDD
<br />13C-2,3,7,8-TCDF
<br />13C-1,2,3,7,8-PeCDF
<br />13C-1,2,3,4,7,8-HxCDF
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />PERCENT
<br />RECOVERY
<br />48
<br />63
<br />68
<br />69
<br />66
<br />46
<br />56
<br />64
<br />66
<br />NOTE (S)
<br />Calculations are pcrfornnd before rounding [o avoid round-off errors in calculated results.
<br />Bold prim deno[es conuul parame[ers
<br />Matrix.........: SOLID
<br />UNITS
<br />P9~g
<br />P4/g
<br />P4/g
<br />P3~g
<br />Pg~9
<br />P9/g
<br />PJ~3
<br />PJ~S
<br />P9~9
<br />Pg/g
<br />PJ~3
<br />P4/~3
<br />PJ~J
<br />Pg~g
<br />P9~J
<br />P9~J
<br />P4/J
<br />PERCENT
<br />RECOVERY
<br />94
<br />101
<br />103
<br />101
<br />103
<br />101
<br />103
<br />96
<br />98
<br />106
<br />96
<br />93
<br />107
<br />100
<br />100
<br />96
<br />93
<br />METHOD
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />SW846 8290
<br />RECOVERY
<br />~~~ ~~~~
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />
<br />14
<br />
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