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<br />BANKS AND GESSO LLC
<br />
<br />Client Sample ID. SAMPLE 1
<br />Trace Level Organic Compounds
<br />Lot-Sample #.-.: D2L050322-001 Work Order #-..: FD97X1AA
<br />Date Sampled...: 11/15/02 13:50 Date Received..: 11/15/02
<br />Prep Date......: 12/11/02 Analysis Date..: 12/14/02
<br />Prep Batch #...: 2345510 Analysis Time_.: 13:46
<br />Dilution Factor: 1
<br />PARAMETER
<br />2,3,7,8-TODD
<br />Total TCDD
<br />1,2,3,7,8-PeCDD
<br />Total PeCDD
<br />1,2,3,4,7,8-HxCDD
<br />1,2,3,6,7,8-HxCDD
<br />1,2,3,7,8,9-HxCDD
<br />Total HxCDD
<br />1,2,3,4,6,7,8-HpCDD
<br />Total HpCDD
<br />OCDD
<br />2,3,7,8-TCDF
<br />Total TCDF
<br />1,2,3,7,8-PeCDF
<br />2,3,4,7,8-PeCDF
<br />Total PeCDF
<br />1,2,3,4,7,8-HxCDF
<br />1,2,3,6,7,8-HxCDF
<br />2,3,4,6,7,8-HxCDF
<br />1,2,3,7,8,9-HxCDF
<br />Total HxCDF
<br />1,2,3,4,6,7,8-HpCDF
<br />1,2,3,4,7,8,9-HpCDF
<br />Total HpCDF
<br />OCDF
<br />INTERNAL STANDARDS
<br />13C-2,3,7,8-TCDD
<br />13C-1,2,3,7,8-PeCDD
<br />13C-1,2,3,6,7,8-HxCDD
<br />13C-1,2,3,4,6,7,8-HpCDD
<br />13C-OCDD
<br />13C-2,3,7,8-TCDF
<br />13C-1,2,3,7,8-PeCDF
<br />13C-1,2,3,4,7,8-HxCDF
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />Matrix_........: SOLID
<br /> DETECTION
<br />RESULT LIMIT UNITS METHOD
<br />ND 0.34 pg/g SW846 8290
<br />ND 0.34 pg/g SW846 8290
<br />ND 0.60 pg/g SW846 8290
<br />ND 0.60 pg/g SW846 8290
<br />ND 0.43 pg/g SW846 8290
<br />ND 0.39 pg/g SW846 8290
<br />ND 0.39 pg/g SW846 8290
<br />ND 0.43 pg/g SW846 8290
<br />ND 0.48 pg/g SW846 8290
<br />ND 0.48 pg/g SW846 8290
<br />ND 2.7 pg/g SW846 8290
<br />ND 0.19 pg/g SW846 8290
<br />ND 0.19 pg/g SW846 8290
<br />ND 0.33 pg/g SW846 8290
<br />ND 0.33 pg/g SW846 8290
<br />ND 0.42 pg/g SW846 8290
<br />ND 0.26 pg/g SW846 8290
<br />ND 0.22 pg/g SW846 8290
<br />ND 0.26 pg/g SW846 8290
<br />ND 0.30 pg/g SW846 8290
<br />ND 0.30 pg/g SW846 8290
<br />ND 0.39 pg/g SW846 8290
<br />ND 0.52 pg/g SW846 8290
<br />ND 0.52 pg/g SW846 8290
<br />ND 0.62 pg/g SW846 8290
<br />PERCENT
<br />RECOVERY
<br />70
<br />82
<br />71
<br />67
<br />62
<br />62
<br />76
<br />70
<br />65
<br />RECOVERY
<br />LIMITS
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />(40 - 135)
<br />7
<br />
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