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Quantitation Report (Not Reviewed) <br />Data Path C: \MSDCI-1EM\2\DATA\ECD"70720\ <br />Data File 020.D <br />Signal(s) Signal ##l: ECDIA.CH Signal #2: ECD2B.CH <br />Acq On 20 Jul 2006 10:24 pm <br />Operator K.Wardzala <br />Sample 06-4523-06G <br />Misc SAMP, 81.51 W, 1, Batch 10409 <br />ALS Vial 20 Sample Multiplier: 1 <br />Integration File signal l: 8151A1.E <br />Integration File signal 2: 8151B1,E <br />Quant Time: Jul 21 09:33:13 2006 <br />Quant Method C:\MSDCHEM\2\METHODS\8151M0718.M <br />Quant Title : ECD7: METHOD SW8151 <br />QLast Update Thu Jul 20 12:47:12 2006 <br />Response via Initial Calibration <br />Integrator: ChemStation 6890 Scale Mode: Small noise peaks clipped <br />Volume Inj. <br />Signal #1 Phase RTx-35 Signal #2 Phase: DB-XLB <br />Signal #1 Info 30M, 0.32 um, 0.2 Signal #2 Info 30M, 0.32 um, 0.5 mm <br />8151M0718.M Fri Jul 21 09:33:14 2006 <br />esponse _ Signal: 020.D1ECD1A.CH <br />4500000 <br />4000000 <br />3500000 \„„,Q <br />~`IJ\Y~ ~Vl/ <br />3000000 ~j `,~ <br />~``~" V ~~ <br />~ <br />2500000 1 ~~} <br />~ V <br />2000000 <br />1500000 <br />1000000 <br />500000 I <br />I <br />I' ~ <br />(I1 <br />~ <br />~ o~, ,y~ <br />r'~ <br /> ~ <br /> <br /> m <br />ime 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 1 .00 13.00 14. 00 15.00 16.00 1 0 ~ <br />esponse Signal: 020.D\ECD2B.CH <br />4500000 <br />4000000 <br />3500000 <br />3000000 <br />2500000 <br />2000000 <br />1500000 <br />1000000 <br />0 <br />500000 0 <br />N ~ <br />O N <br />N`P f <br />0 ~ ti_ <br /> C <br />O ~ N ~ iC <br /> <br /> <br />ime <br />1.00 2.00 <br />3.00 4.00 ~~ <br />5.00 6.00 7.00 8.00 9.00 10.00 11.00 12 00 13 00.14.00 15.00 16.00 17.00 <br />Page: 2 <br />• <br />• <br />i <br />