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Evergreen Analytical, Inc. <br />Work Order: OS-9449 <br />Client Project ID: Lupton Lakes <br />Date: 09-Jan-06 <br />ANALYTICAL QC SUMMARY REPORT <br />BatchlD: 8954 <br />Sample ID: MB-8954 SampType: MBLK TestCode: 6020_D Run ID: ICPMS_051229A Prep Date: 12/28/05 Units: mgtL <br /> Batch ID: 8954 TestNo: SW6020 FileID: 051229A.B\016SMPL.D Analysis Date: 12/29/05 SegNo: 395268 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Arsenic U 0.0020 <br />Calcium U 0.40 <br />Iron U 0.20 <br />Magnesium U 0.030 <br />Sodium U 0.50 <br />Sample ID: 05-9449-01DPDS SampType: PDS TestCode: 6020_D Run ID: ICPMS_051229A Prep Date: 12/28/05 Units: mgtL <br />Client ID: CRMW-07 Batch ID: 8954 TestNo: SW6020 FileID: 051229A.B1022SMPL.D Analysis Date: 12/29/05 SegNo: 395273 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Arsenic 0.241 0.0020 0.25 0 96.4 75 125 0 0 <br />Calcium 87.8.5 0.40 2.5 83.8 162 75 125 0 0 S ~'- <br />Iron 2.996 0.20 2.5 0.63 94.6 75 125 0 0 <br />Magnesium, 21.35 0.030 2.5 18.8 102 75 125 0 0 <br />Sodium 117.4 0.50 2.5 115.5 76 75 125 0 0 <br />Sample ID: LCS-8954 SampType: LCS TestCode: 6020_WT Run ID: ICPMS_060103A Prep Date: 12/28/05 Units: mg/L <br /> Batch ID: 8954 TestNo: SW6020 File(D: 060103A.B102iSMPL.D Analysis Date: 1/3/06 SegNo: 395877 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Arsenic 0.3 0.0020 0.3 0 100 80.3 110 0 0 <br />Calcium 3.291 0.40 3 0 110 88 116 0 0 <br />Iron 3.123 0.20 3 0 104 ' 86.4 116 0 0 <br />Magnesium 3.256 0.030 3 0 109 83.2 123 0 0 <br />Sodium 3.161 0.50 3 0 105 77.9 122 0 0 <br />~ ~/ ~ R 4 ~~- rQb `~ ~/ CSAr7/~ t!6 -f- S r (~~ j O,Z ~~ <br />Qualifiers: ND -Not Detected at the Reporting Limit R -RPD outside accepted recovery limits <br />I -Analyte detected below quantitation limits B -Analyte detected in the associated Method Blank <br />S -Spike Recovery outside accepted recovery limits ti -Sample exceeded analytical holding time Print Date: 1/9/06 <br />