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2.0 METHODS <br />Each area to be sampled was delineated on a recent Seneca Coal photobase map. All <br />sample locations were randomly selected and geographically distributed across each area. <br />Soil backhoe pits were located and dug to at least five feet by Seneca Coal. A composite <br />sample of each appropriate depth interval was collected at each pit location. Samples <br />were screened in the field over a No.10 (2mm) screen to remove the much larger, hard <br />rocks, and the percent coarse fragments (gravel, cobble, and boulder size rock material) <br />was estimated and recorded on the profile description form. Sample depth was noted for <br />each location as well as other pertinent information. <br />In addition to soil sampling, a complete soil profile description was completed at each <br />backhoe pit location. Soils description followed standard Natural Resources <br />Conservation Service (NRCS) field methods (Schoeneberger et.al., 2002). Digital <br />photographs were taken of each pit and adjacent landscape. All soil and spoil laboratory <br />data was reviewed and approved by IML soils laboratory supervisor Ms. Karen Secor. <br />All soil and spoil samples were analyzed by IML. The analytical parameters for the soil <br />backhoe pits included: pH; saturation percent, electrical conductivity (EC); sodium <br />adsorption ratio (SAR calculation from meq/L for calcium, magnesium, and sodium); <br />texture (percent sand, silt, and clay - by hydrometer method), and NPK (nitrate-nitrogen, <br />phosphorus, and potassium, ppm). The overburden spoil samples from the backhoe pits <br />were also analyzed for these parameters, except for phosphorus and potassium, as well as <br />Boron (B), Selenium (Se), and acid-base potential (ABP) which included separate <br />analysis/calculation for total sulfur percent, total sulfur acid-base (tons/1000 tons), <br />neutralization potential (tons/1000 tons), and total sulfur acid-base potential (tons/1000 <br />tons). None of the spoil samples needed the additional pyritic sulfur acid-base potential <br />(tons/1000 tons) analysis (sulfur fractionation) which is routinely run for any samples <br />with a total sulfur ABP of less than minus five (<5.0). <br />All field and laboratory data were evaluated for "suitability" based on standard threshold <br />values for significant parameters, primarily EC, SAR, and AB potential. References for <br />suitability evaluation include "Criteria for Evaluating Overburden, Underburden, and <br />Regraded Spoil Suitability" (Seneca Coal IIW Mine, Table 6-3, revised January 2002), <br />and "Criteria to Establish Suitability of Topsoil, or Topsoil Substitutes, and Overburden" <br />(Wyoming Department of Environmental Quality, Tables I-2 and I-4, revised <br />November1996). Unsuitable values include pH (<5 or >9), saturation percent (<25 or <br />>85), electrical conductivity (EC>12), sodicity (SAR >18 or >22 depending on percent <br />clay content), and nitrate-nitrogen (>60ppm). Clay, sandy clay, or silty clay texture with <br />greater than 50 percent clay content is also considered unsuitable except with <br />amelioration (Seneca Coal IIW Mine, 2002). <br />3.0 RESULTS <br />• Reapplied Topsoil/Overburden Spoil (Backhoe Pits) Laboratory Results• <br />l <br />2 <br />