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Evergreen Analytical, Inc. <br />Work Order: 07-4617 <br />Client Project ID: Last Chance <br />Date: 03-Aug-07 <br />ANALYTICAL QC SUMMARY REPORT <br />BatchID: 13180 <br />Sample ID: MB-13180/13116 SampType: MBLK TestCode: SPLPMETAL Run ID: ICP-OPTIMA 5300 DV_070801A Prep Date: 8/1/07 Units: mg/L <br /> Batch ID: 13180 TestNo: SW1312/6010 FileID: 080107PM Analysis Date: 8/1/07 SegNo: 590951 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Aluminum U 0.11 <br />Arsenic U 0.15 <br />Barium 0.0401 0.0050 <br />Cadmium U 0.0050 <br />Chromium U 0.050 <br />Copper U 0.015 <br />Iron U 0.35 <br />Lead U 0.37 <br />Molybdenum U 0.025 <br />Nickel U 0.010 <br />Selenium U 0.50 <br />Silver U 0.023 <br />Uranium U 1.9 <br />Vanadium U 0.050 <br />Zinc U 0.056 <br />Sample ID: 07-4879-01AMS SampType: MS TestCode: SPLPMETAL Run ID: ICP-OPTIMA 5300 DV_070801A Prep Date: 8/1/07 Units: mg/L <br /> Batch ID: 13180 TestNo: SW1312/6010 FileID: 080107PM Analysis Date: 8/1/07 SegNo: 590937 <br />Analyte Result LOL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Arsenic 1.041 0.15 1 0 104 50 150 0 u <br />Barium 6.359 0.0050 5 0.8761 110 50 150 0 0 <br />Cadmium 0.5159 0.0050 0.5 0 103 50 150 0 0 <br />Chromium 5.259 0.050 5 0 105 50 150 0 0 <br />Lead 2.368 0.37 2 0 118 50 150 0 0 <br />Selenium 3.025 0.50 3 0 101 50 150 0 0 <br />Silver 0.4874 0.023 0.5 0 97.5 50 150 0 0 <br />Qualifiers: U -Not detected at or above the Reporting Limit R -RPD outside acceptance limits <br />J -Analyte detected below quantitation limits B -Analyte detected in the associated Method Blank <br />S -Spike Recovery outside acceptance limits H -Prep or analytical holding time exceeded <br />E -Extrapolated value, value exceeds calibration range. X -See case narrative <br />