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Evergreen Analytical, Inc. <br />Date: 06 Aug-07 <br />work Order: 07-4617 ANALYTICAL QC SUMMARY REPORT <br />Client Project ID: Last Chance <br />TestCode: ANIONS S <br />Sample ID: MB-R33240 SampType: MBLK TestCode: ANIONS_S Run ID: IC-DX120_070730A Prep Date: 7/30/07 Units: mg/Kg <br /> Batch ID: R33240 TestNo: E300.0 FileID: Analysis Date: 7/30/07 SegNo: 589989 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br />Nitrite-N U 0.0040 <br />Nitrate-N U 0.010 <br />Nitrite+Nitrate-N U 0.013 <br />Sulfate U 0.50 <br />Sample ID: LCS-R33240 SampType: LCS TestCode: ANIONS_S Run ID: IC-DX120_070730A Prep Date: 7/30!07 Units: mg/Kg <br /> Batch ID: R33240 TestNo: E300.0 FileID: Analysis Date: 7/30/07 SegNo: 589990 <br />Analyte Result LQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val °RPD RPDLimit Qual <br />Nitrite-N 6.112 0.0080 6.09 0 100 90 110 0 0 <br />Nitrate-N 4.572 0.020 4.518 0 101 90 110 0 0 <br />Nitrite+Nitrate-N 10.68 0.026 10.61 0 101 90 110 0 0 <br />Sulfate 30.23 1.0 30 0 101 90 110 0 0 <br />Sample ID: U7~617-01AMS SampType: MS TestCode: ANIONS_S Run ID: IC-DX120_070730A Prep Date: 7/30/07 Units: mg/Kg <br />Client ID: WASTE Batch ID: R33240 TestNo: E300.0 FileID: Analysis Date: 7/30/07 SegNo: 589993 <br />Analyte Result LQL SPK value SPK Ref Val °REC LowLimit .HighLimit RPD Ref Val °hRPD RPDLimit Qual <br />Nitrite-N 34.16 0.040 30.45 2.979 102 75 125 0 0 <br />Nitrate-N 47.6 0.10 22.59 22.22 112 75 125 0 0 <br />Nitrite+Nitrate-N 81.75 0.13 53.04 25.2 107 75 125 0 0 <br />Sulfate 162.5 5.0 100 54.66 108 75 125 0 0 <br />Qualifiers: U -Not detected at or above the Reporting Limit R -RPD outside acceptance limits <br />J - Analyte detected below quantitation limits B - Analyte detected in the associated Method Blank <br />S -Spike Recovery outside acceptance limits H -Prep or analytical holding time exceeded <br />E -Extrapolated value, value exceeds calibration range. X -See case narrative <br />