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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800) 334-5493 <br />L55740-01 WG203963 Selenium, potentially dissolved M200.8 ICP-MS <br />WG203926 Cyanide, WAD SM4500-CN I-Colorimetric w/ <br />distillation <br />WG203865 Residue, Non-Filterable (TSS) @105C M160.2 - Gravimetric <br />L55740-02 WG203888 Iron, dissolved <br />L55740-04 WG203904 Arsenic, total <br />Cadmium, total <br />WG203979 Manganese, potentially dissolved <br />WG204014 Cyanide, total <br />WG204034 Phosphorus, total <br />WG203865 Residue, Non-Filterable (TSS) @105C <br />M200.7 ICP <br />M200.8 ICP-MS <br />M200.8 ICP-MS <br />M200.7 ICP <br />M335.4 - Colorimetric w/ <br />distillation <br />M365.1 -Auto Ascorbic Acid <br />(digest) <br />M160.2 - Gravimetric <br />M1 Matrix spike recovery was high, the method control sample <br />recovery was acceptable. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />M3 The accuracy of the spike recovery does not apply because <br />analyte concentration in the sample is disproportionate to <br />the spike level. The recovery of the method control sample <br />was acceptable. <br />M3 The accuracy of the spike recovery does not apply because <br />analyte concentration in the sample is disproportionate to <br />the spike level. The recovery of the method control sample <br />was acceptable. <br />M3 The accuracy of the spike recovery does not apply because <br />analyte concentration in the sample is disproportionate to <br />the spike level. The recovery of the method control sample <br />was acceptable. <br />MA Recovery for either the spike or spike duplicate was outside <br />of the acceptance limits; the RPD was within the <br />acceptance limits. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low far <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />REPAD.15.06.05.01 <br />L55740: Page 9 of 13 <br />Climax Mine ACZ Project ID: L55740 <br />