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V+/td/I{ {\r{• <br /> <br />yrwa ra• ••a• aa~t rnawurt.x «• r a awe fun6/07a . <br />n <br />A E C I <br />fie potential for wch aMacts wax pardalry tacapnlaed, aibah aomawnat after ttw analyak, <br />by AeevLaha. Thar dawnpraded their priplNl utlmau of 0.07 t mp/L eYanlda t0 0.006 <br />mc1l. the detection Amk for heal solutlona, N the Apdt 1, t oY1 lyeimatar pmpia, <br />It k beAawd, bawd on tna aample rttatrla and ale, that N anY eyantde oeeurnd In th <br />lyiimatar L] umplaa, h eould M nehhar dataaad nor qu^rttifl.d by the atrtaanalywr <br />taehnique at lawla below a minimum o? 0,02 mp/L. h h worth notlno thtt >nk 1. the <br />ganuutlon limit wad by anotlur Danwr laboratory tar thalr atttaanalyaN tYanlda anahnh, <br />without at:countlnp }or aawn matrix aHaota. <br />J.6 Abuna of Qusllty Aatugnca <br />3.6.1 Laboratory dA prooaduru <br />Ouallty aswranaa (~Al procaduna en Oatipnad to utlmap, atCOlrnt for and allntMat~ <br />analytieal error in the laboratory In the enalyala of aamplaa. ThU la tchiawd by anslyahtl <br />nplinua of sample to auau nproduolbility, and 'aplkinp' aamplaa with known addhbM <br />of the apeclaa belno enalvaad, to sooount for tM attacu the matrl: mtpht haw on tM <br />malya4, <br />3,6.4 Lyslmaur L3 aamplaa <br />N(th rrapact SO the tyaimatar L3 umplaa tM following Comment. On 4A progduna can ba <br />made; <br />' aampla 12118182: n0 Internal W wax run m thla aampla due to the limited aampla <br />volume. Therefore, the effecn of matrix intartaranca were not aaaeseed; <br />• umpls 02121/82: umpla L3WT21, the aampla from the L9 lytlmeter, wet neaiwd part <br />the holc~np time for pynnida arutytla. VJhila CA rep!~cePcn a,. tPiii^'v weteccl wan ueaC <br />w::n in''a tamPle ht:C ~, [h{ II CCr I: Pry er.Cla Ira n_P Y.:r, •e .ec~~itdl, ine Qiipnlt ad wa'!r <br />L i^. !V CA e~a~de;~c^. a^,! nscc• p~tS n..^t r. tutu :rat rnn• r tr'rcu en ir•t 2G ml a~ra <br />' temple 04!03,'92: rti,tn only b mu of tempo. Iharr wn intvHicam c4mpia to pa:Yorm Q/. <br />pr OCadUraa on ihle Da RiCUler urn pla. In adtlrt.Dn, tn1 rat; a'tact 01 puttlnp $ pram! Of <br />aodlum nydroxlde Into the 6 m4 of aampla would have ratuhed In 'dllutlon' of ine aample <br />volume, wnleh would ruult ~n daucfion limp In Ina actual temple ba!^q nigher than <br />Inttrumantal drtactlpn Ilmita In tM laboratory. <br />