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PROCEDURE FOR DETEP`4INATION OF <br />0.3 AND 15 ATMOSPHERE PRESSURE POINT <br />1. Preparatory Steps: <br />a. Sieve soil samples through a 8 mesh screen. <br />b. Pre-soak the porous plate for 2 hours inside the <br />pressure chamber. <br />2. Procedure for setting up the pressure chamber: <br />a. Place the sample. retainer rings on the porous plate. <br />b. Pour a soil sample into each rings, level with the top. <br />c. Allow the samples to stand at least 16 hours with <br /> an excess of water on the plate. <br />3. At 8:00 a.m. the following day: <br />a. Remove excess water fro-i the membrane with a pipet <br /> or rubber syringe. <br />• b. Close the pressure membrane apparatus and admit air <br /> to the soil chamber at a pressure of 1/3 atmosphere <br /> (5 p.s.i.). When running 15 atmosphere pressure <br /> point apply a pressure of 15 atmosphere (220 p.s.i.). <br />c. Remove the samples when the readings on an outflow <br />buret indicate equilibrium has been attained. Some <br />soils will approach equilibrium in 18 to 20 hours. <br />d. Before releasing the ai= pressure in the pressure <br />cooker, put a pinch claap on the outflow tube on <br />each plate. This prevents backflow of water to the <br />samples after the pressure is released. <br />e. To avoid changes in the moiiture content of the <br />samples, transfer the samples quickly to previously <br />weighed soild moisture cans. <br />f. Determine the moisture content by drying to constant <br />weight at 105°C. Express the moisture content as <br />percent, dry weight basis. <br />4. Calculate ~ moisture remaining after 1/3 atmosphere or 15 <br />atmosphere• <br />a. Subtract oven-dry weight of soil plus can from moisture <br />weight of soil plus'can. This gives weight of water <br />remaining after 15 atmosphere pressure. <br />b. Subtract weight of can`_ron oven-dry weight of soil <br />plus can. <br />6-68 <br />