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TABLE 6-2A <br />Parame~[er, Procedure, and Reference List <br />for Seneca llW-Southern Mine Block Overburden Analysis <br />by InterMountain Lab, Sheridan, Wyoming, April 1992 <br />Parameter-Units Procedure-Reference <br />Sample Preparation Samples were dried at less than 35°C and crushed <br />to pass a 10 mesh sieve (excessive grinding was <br />avoided). <br />Subsampling less than 2 mm fraction USDA 119691. Method 1, p. 83-84. <br />Preparation of saturation extract and saturation Rhoades 119821, Method 10-2.3.1. <br />percentage determination <br />pH (determination using saturated pastel <br />Conductivity of saturation extract in mmhos/cm at <br />25°C <br />Soluble calcium, magnesium, and sodium in meg/1 <br />Sodium Adsorption Ratio <br />Particle size analysis in % sand, silt, and clay <br />Sand Fractionation in % <br />Total sulfur in % <br />Sulfur fractionation in % <br />Neutralization potential in tons CaCO~ per 1,000 tons <br />of spoil <br />Acid base potential (APBI in tons CaCO~ per 1,000 <br />tons of spoil <br />Manganese in ppm <br />Molybdenum in ppm <br />Cadmium, Copper, Nickel, Arsenic, Chromium, Lead, <br />and Zinc in ppm <br />Iron in ppm <br />Selenium in ppm <br />Mercury in ppm <br />Boron in ppm <br />Chlorine and Fluorine in ppm <br />Aluminum in ppm <br />Ammonium- and Nitrate-Nitrogen in ppm <br />USDA (19691. Method 21a, p. 102. <br />Rhoades 119821, Method 10-3.3. <br />Rhoades 11982), Section 10-3.4. <br />USDA 11969), p. 26. <br />Gee and Bauder 119861, Method 15.5. <br />Gee and Bauder 119861, Method 15-5.2.4. <br />Sobek et al. 119781, p. 51.55, 60 mesh sieve. <br />ASTM (19801, 60 mesh sieve. <br />USDA (1969) Method 23C, p. 105, 60 mash sieve. <br />Smith et al. 119741, p. 48-49, 60 mesh sir:ve. <br />Gambrel) and Patrick 119821, Method 18-3.4. <br />Vlek (19751, extraction by NH,CO~ or Reisenauer <br />(19651. Section 74-2.3. <br />Baker and Amacher (19821. Method 19-3.:3. <br />Olson and Ellis 119821, Method 17-4.3. <br />Fine (1965), Method 80-3 and Soltanpour et al. <br />(1982), Method 3-5.5.4. <br />Stewart and Bettany 119821, Method 22-3. <br />Bingham (19821, Method 25-9.1. <br />Adriano and Doner 119(321. Methods 26-3 ,and 26- <br />4.4. <br />Barnhisel and Bertsch 119821, Method 16-3.2. <br />Keeney and Nelson 119821, Methods 33-6.2 and 33- <br />6.3 or 33-7 and 33-8. <br /> <br />• <br /> <br />22 Revised 9/98 <br />