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Qrder # 96-03-054 City of Boulder Wastewater TP <br />ANALYTICA, INC. TEST METHODOLOGIES <br />THE FOLLOWING CODES APPLY TO THE ANALYTICAL REPORT <br />Page 6 <br />RESULT field... <br />ND = not detected at the reported limit <br />NA =analyte not applicable (see case narrative/methods for ~iiscussion) <br />Q (qualifier) field... <br />GENERAL: <br />* = Recovery or BRPD outside method specifications <br />H = value is estimated due to analysis run outside EPA holdin~~ times <br />E = reported concentration is above the instrument calibratio;z range <br />D = analyte was diluted to bring within instrument calibratio;a range or <br />to remove matrix interferences <br />ORGANIC ANALYSIS DATA QUALIFIERS: <br />B = analyte was detected in the laboratory method blank <br />J = analyte was detected above the instrument detection limit (IDL) <br />but below the analytical reporting limit (CRDL) <br />INORGANIC ANALYSIS DATA QUALIFIERS: <br />B = analyte was detected above the instrument detection limit (IDL) <br />but below the analytical reporting limit (CRDL) <br />A = post digestion spike did not meet criteria (70-1308), therefore the <br />reporting limit was raised by a factor of two to reflect spike failure <br />S = reported value determined by the Hethod of Standard Additions <br />