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PERMFILE109666
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PERMFILE109666
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Last modified
8/24/2016 10:06:42 PM
Creation date
11/24/2007 6:41:15 PM
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Template:
DRMS Permit Index
Permit No
C1981008A
IBM Index Class Name
Permit File
Doc Date
12/11/2001
Section_Exhibit Name
NH1 TAB 6 APPENDIX 6-3 CHEMICAL ANALYSIS PROCEDURES
Media Type
D
Archive
Yes
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DETERMINATION OF AVAILABLE POTASSIUM, CALCIUM, <br />MAGNESIUM, A[JD SODIUM IN SOILS <br />Montana State University - College of Agriculture <br />Stock Solutions: <br />Potassium - 1000ppm: Weigh b.9066g of pure dry (1 hour in oven <br />at 105 C) KC1 into liter volumetric flask, <br />add distilled-deionized water to dissolve, <br />then bring to volume with distilled-deionized <br />water. <br />Sodium - 1000ppm: Weigh d1.5421g of pure dry (1 hour in oven <br />_._.._ at 105 ) NaCl into a liter volumetric <br />flask, add distilled-deionized water to <br />dissolve, then bring to volume with <br />distilled-deionized water. <br />Ammonium Acetate-1N: Weigh 154.16g of ammonium acetate (pH7) <br />into a 2 liter volumetric flask and dilute <br />to volume with distilled-deionized water. <br />• Standard Solutions: <br />200ppm Potassium: Pipet 100m1 of 1000ppm K stock solution <br />into SOOml volumetric flask, then bring <br />to volume with 1N NH4OAC. (Ammonium <br />acetate extracting solution) <br />200ppm Sodium: Pipet 100m1 of 1000ppm Na stock solution <br />into SOOml volumetric flask, then briny <br />to volume with 1N NH4OAC. <br />PROCEDURE FOR ANALYZING SOILS SAMPLES <br />1. Weigh 2.Sg of soil into 250m1 erlenmeyer flask. <br />2. Add SOml of 1N ammonium acetate extracting solution. <br />3. Shake the soil on mechanical shaker for 30 minutes. <br />4. Centrifuge the extract until clear. <br />5. An aliquot of extract is diluted to volume, with the final <br />volume 1% SrC12. ~ <br />6. Analyze directly for Ca, Na, P~Ig, & K directly on Perkin-F.lmer <br />• Atomic Absorption Spectrophotometer. <br />The dilution required will depend upon the type of soil analyz•~d. <br />It is important to match the % SrCl2 in both standards and samples. <br />6-n5 <br />
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