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Date: 19-Jul-00 <br /> Barringer Laboratories, Inc. RUN QC SUMMARY REPORT <br /> 15000 W 6th Avenue Suite 300 Golden,Colorado 80e01-5047 (800)654-0506 (303)277-1687 Fax(303)277-1689 <br /> lient: CGRS Run ID: ICAP 000705A Sample ID: ICB Method: SW8466010B Prepped: <br /> Jork Order: 0006205 — SegNo: 151476 Unit: mglL Analyzed: 7/5100 <br /> roject: 1-135-2755 Initial Calibration Blank Matrix: Aqueous Analyst: SLM <br /> nalyte Result 12 sigma Limit SpikeVal SpikeRefVal %REC Lowl-imil HighLimit DupRefVal t 2 sigma RPD/RER RPDLimit Qual <br /> olybdenum,total NO 0.01 <br /> lient: CGRS Run ID: ICAP_000705A Sample 10: ICSAI Method: SW8466010B Prepped: <br /> Jork Order: 0006205 SegNo: 151477 Unit: mg/L Analyzed: 715/00 <br /> roject: 1-135.2755 Interference Check Sample A Matrix: Aqueous Analyst: SLM <br /> nalyte Result x 2 sigma Limit SpikeVal SpikeRefVal %REC Lowl-imit HighLimit DupRefVal t 2 sigma RPD/RER RPDLimit Qual <br /> olybdenum, total NO 0.01 NO 0 0 0 <br /> ient: CGRS Run ID: ICAP 000705A Sample ID: ICSABI Method: SW8466010B Prepped: <br /> Jork Order: 0006205 SegNo: 151478 Unit: mg/L Analyzed: 715100 <br /> roject: 1-135.2755 Interference Check Sample AB Matrix: Aqueous Analyst: SLM <br /> nalyte Result t 2 sigma Limit SpikeVal SpikeRefVal %REC Lowl-imit HighLimit DupRefVal t 2 sigma RPD/RER RPDLimit Qual <br /> olybdenum,total NO 0.01 ND 0 0 0 <br /> ient: CGRS Run ID: [CAP 000705A Sample ID: 0006200-01APDS Method: SW8466010B Prepped: <br /> fork Order: 0006205 SegNo: 151485 Unit: mg/L Analyzed: 7/5/00 <br /> roject: 1.135-2755 Post Digestion/Distillation Spike Matrix: Aqueous Analyst: SLM <br /> nalyte Result t 2 sigma Limit SpikeVal SpikeRefVal %REC Lowl-imil HighLimit DupRefVal t 2 sigma RPD/RER RPDLimit Ou <br /> olybdenum, total 2.1 0.02 2.0 0.030 104 75 125 <br /> ient: CGRS Run ID: ICAP_000705A Sample ID: CCV1 Method: SW8466010B Prepped: <br /> fork Order: 0006205 SegNo: 151487 Unit: mg/L Analyzed: 715100 <br /> roject: 1.135.2755 Continuing Calibration Verification Matrix: Aqueous Analyst: SLM <br /> nalyte Result t 2 sigma Limit SpikeVal SpikeRefVal %REC Lowl-imit HighLimit DupRefVal t 2 sigma RPD/RER RPDLimit Quit <br /> olybdenum, total 5.3 0.01 5.0 106 90 110 <br /> ient: CGRS Run ID: ICAP_000705A Sample ID: CCB1 Method: SW8466010B Prepped: <br /> Jork Order: 0006205 SegNo: 151488 Unit: mg/L Analyzed: 715100 <br /> roject: 1.135-2755 Continuing Calibration Blank Matrix: Aqueous Analyst: SLM <br /> nalyte Result t 2 sigma Limit SpikeVal SpikeRefVal %REC Lowl-imit HighLimit DupRefVal s 2 sigma RPD/RER RPDLimit Quat <br /> olybdenum, total NO 0.01 <br /> Qualifiers: NO-Not detected at the reporting limit R-RPD outside accepted recovery limits Y-Unspiked sample>4 times amount spiked <br /> J-Analyte detected below quantitation limit X-Duplicate sample(s)<5 times limit B-Analyte detected in the associated method blank <br /> E-Value above quantitation range S-Spike recovery outside accepted recovery limits Z-Sample> 10 limes blank result Page 21 of 29 <br />