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VIIIB. INORGANIC ANALYSIS WORKSHEET -FURNACE AA ANALYSIS <br />TECHLAW <br />BATCH: 1.6 ~ZZ2 <br />If the sample result is > = 50 % of the spike result and the percent rewvery was between 40$4 % or> 115°,6, then MSA must be <br />pedormed. <br />upl au SLIrIp ICS Ior wruUl Cn rvwn Cualy>p wG> ley WfCU uul WI penuluieu, ul mJH m>wu wne uulslae ConllOl IIn IIIS. <br />isl Corr. 2nd Com. <br />Analyte Sample ID CceH. CoeH. Action Comments <br />i. Estimate (J) A an MSA was required and not performed. <br />2 If the correlation coefficient was <0.995, the MSA shoultl be performed a second time. Estimate (J) all sample results. r <br />If a reanalysis was not peformed, or the reanalysis correlation coefficient was <0.995, or result hom the highest wrrelalion coefficient was not <br />reportetl. <br />List all sample > CRDL whose duplicate injections did not agree within 20% RSD ar CV, or samples in which duplic: to injections were not <br />performed. <br />Sample Duplicate ° <br />Analyte Sample ID Result Result /0 RSD or CV CRDL Action Comment <br />spike reswt = IsplKec sample resun -sample resmq <br />Actions: <br />t. Estimate (J) detected results greater than the CRDL if duplicate injections are outside 20 % RSD. <br />2 Estimate (J) all sample results i(duplicate infections were not pedormed <br />NOTE. Three separate spiked sample concentration levels, in addition to the unsprRed sample must be analyzed for each MSA. <br />Inorg98.xls <br />