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<br />~; <br /> <br />1 <br />1 <br /> <br /> <br /> <br />i> <br />1 <br /> <br /> <br /> <br /> <br />TABLE 7 - METHOD 1312 PRECISION RESULTS FOR VOLATILES <br />Soil No. 1 <br />(Western) <br />Compound Name <br />Acetone <br />Acrylonitrile <br />Benzene <br />n-Butyl Alcohol <br />(1•Butanol) <br />Carbon disulfide <br />BReg.* BRSD <br />44.0 12.4 <br />52.5 68.4 <br />47.8 8.29 <br />55.5 2.91 <br />21.4 16,4 <br />Carbon tetrachloride <br />Chlorobenzene <br />Chloroform <br />1,2-Dichloroethane <br />1,1-Dichloroethane <br />Ethyl acetate <br />Ethylbenzene <br />Ethyl ether <br />Isobutanol (4-Methyl <br />-1-propanol) <br />Methylene chloride <br />Methyl ethyl ketone <br />(2-Butanone) <br />Methyl isobutyl <br />ketone <br />1,1,1,2-Tetrachloro- <br />ethane <br />1,1,2,2-Tetrachloro- <br />ethane <br />Tetrachloroethene <br />Toluene <br />1,1,1-Trichloro- <br />ethane <br />1,1,2-Trichloro- <br />ethane <br />Trichloroethene <br />Trichloro- <br />fluoromethane <br />1,1,2-Trichloro- <br />trifluoroethane <br />Vinyl chloride <br />40.6 18.6 <br />64.4 6.76 <br />61.3 8.04 <br />73.4 4.59 <br />31.4 14.5 <br />76.4 9.65 <br />56.2 9.22 <br />48.0 16.4 <br />0.0 ND <br />47.5 30.3 <br />56.7 5.44 <br />81.1 10.3 <br />69.0 6.73 <br />85.3 7.04 <br />45.1 12.7 <br />59.2 8.06 <br />47.2 16.0 <br />76.2 5.72 <br />54.5 11.1 <br />20.7 24.5 <br />18.1 26.7 <br />10.2 20.3 <br />' * Triplicate analyses <br />** Six replicate analyses <br />*** Five replicate analyses <br />1 <br />1~ <br />1 <br />Soil No• <br />(Eastern) <br />c <br />lRe <br />.* >4RSD <br />43.8 2.25 <br />50.5 70.0 <br />34,8 16.3 <br />49.2 14.6 <br />12.4 49.5 <br />22.3 29.1 <br />41.5 13.1 <br />54.8 16.4 <br />68.7 11.3 <br />22.9 39.3 <br />75.4 4.02 <br />23.2 11.5 <br />55.1 9.72 <br />0.0 ND <br />42.2 42.9 <br />61.9 3.94 <br />88.9 2.99 <br />41.1 11.3 <br />58.9 4.15 <br />15.2 17.4 <br />49.3 10.5 <br />33.8 22.8 <br />67.3 8.43 <br />39.4 19.5 <br />12.6 60.1 <br />6.95 58.0 <br />7.17 72.8 <br />1312 - 21 <br />Soil No. 3_ <br />(Western and <br />Sludge) <br />g <br />BRe <br />.** 9RSIi <br />116.0 11.5 <br />49.3 44.9 <br />49.8 36.7 <br />65.5 37.2 <br />36.5 51.5 <br />36.2 41.4 <br />44.2 32.0 <br />61.8 29.1 <br />58.3 33.3 <br />32.0 54.4 <br />23.0 119.8 <br />37.5 36.1 <br />37.3 31.2 <br />61.8 37.7 <br />52.0 37.4 <br />73.7 31.'.3 <br />58.3 32.ii, <br />50.8 31.'i <br />64.0 25.1 <br />26.2 44.0 <br />45.7 35.2 <br />40.7 40.t~ <br />61.7 28.11 <br />38.8 40.5 <br />28.5 34.0 <br />21.5 67.8 <br />25.0 61.0 <br />Soil No. 4 <br />(Western and <br />Sludge) <br />o <br />BRe <br />. *** 9RSD <br /> <br />21.3 71.4 <br />51.6 4.6 <br />33.4 41.1 <br />73.0 13.9 <br />21.3 31.5 <br />24.0 34.0 <br />33.0 24.9 <br />45.8 38.6 <br />41.2 37.8 <br />16.8 26.4 <br />11.0 115.5 <br />27.2 28.6 <br />42.0 17.6 <br />76.0 12.2 <br />37.3 16.6 <br />40.6 39.0 <br />39.8 40.3 <br />36.8 23.8 <br />53.6 15.8 <br />18.6 24.2 <br />31.4 37.2 <br />26.2 38.8 <br />46.4 25..4 <br />25.6 34.1 <br />19.8 33.9 <br />15.3 24.8 <br />11.8 25.4 <br />Revision 0 <br />November 1990 <br />