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i~ <br />1 <br />1 <br />1 <br />1 <br />1 <br />~,I,~ <br />Western Atlae <br />Inter~atianal <br />o..~cv. <br />CORE LABORATORIES <br />1 T L E <br />SOP ND. <br />ANALYTICAL CHEMISTRY DIVISION QUALITY ASSURANCE MANUAL <br />HC-QAC-02 <br />REVISION N0. (EFFECTIVE GATE (PAGE <br />0 I 1 /06/92 I 89 of 1 <br />• Compare raw laboratory data documentation to the data entered in LIMS <br />for several parameters. <br />• Spot-check data calculations, dilution factors, etc. for several different <br />parameters. <br />• Verify that the required data review and validation documentation is <br />present. <br />14.5 Final Report Review And Approval <br />Laboratory section supervisors, project managers, the QA/Q~ coordinator, or <br />the laboratory manager are responsible for approving the final reportable <br />package which is delivered to the client. The following items must be verified <br />before releasing the final analytical and quality assurance reports. <br />• Final analytical report format and content is appropriate amd meets client <br />and regulatory requirements. <br />• Review the final analytical and quality assurance reports to assure that the <br />data reported is correct (significant figures, method references, detection <br />limits, units, and date and time analyzed). <br />• Verify that any additional quality assurance reportables requested by the <br />client are provided (matrix spike duplicates, copies of raw lab data, <br />surrogate recoveries, etc.) <br />• Analytical and quality assurance problems associated with that job are <br />documented and included in both the job file and final report, when <br />necessary. <br />• Decisions made to report data which deviates from method-specified <br />requirements are documented and included in both the job file and final <br />report. <br />• Analytical and quality assurance problems are addressed arid appropriate <br />corrective action is taken and documented to minimize or eliminate the <br />problem. <br />