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ACZ Laboratories, Inc. ~ ' - <br />' 2773 Downhill Dme Steamboat Springs, CO 80487 (B00) 3345493 <br />' .Batch A distinct set of samples analyzed at a spedfic tlma <br />Found Value of the CC Type of interest <br />Limit Upper limit fw RPD, in %. <br />Lower Lower Recovery Limit, in % (except for LCSS, ng/f~) <br />MDL Method Detection Limit Same as Minimum Reporting Limit Allows fw ktsW merit and annual OucWatlons. <br />PCNISCN~ A rwmbw assigned m reagentslsUndartls to Voce to the manufacture/s cenifiate of anaysis <br />PDL Wadicel Duantitagon UmiL typinlly 5 8mes Me MDL. <br />' QC Tnre Value of the Conbd Sample w the amwnt added b the Sp&e <br />Rec Amours of the true value w spike added recovereq in % (except fw LOSS. rrgMg) <br />RPD RehGve Percem Dgference. Calculation used fw Wplicate llC Types <br />Upper Upper Recovery Limi[, in % (except for LCSS, mg/Kg) <br />. Semple Value of the Sampe of interest <br /> • <br />AS Anaytictl Spike (Past Digestion) LCSWD Laboratory Control Sample -Water Duplicate <br />ASD Anatyficel Spike (Post Digeston) Duplkate LFB Latxxatory Fwgfied Blank <br />CCB CanBnuing CaGLvation Blank 1FM lalwraiory Fortified Matrix <br />CCV Contlnuing Cafivation Verification standard IFMD Labomtory Fortified Mam% Dupfipte <br />Df/P Sample Dupficete LRB Laboratory Reagent Blank <br />ICB Initial Calibration Blank MS Matrix Spike <br />ICV lrttgal CaGbratbn Verification standard MSD Matrix Spike Duplicere <br />ICSAB Interelerttent l.wredion StarMard - A dus B sdutkxu PBS Prep BWnk - Shc <br />LCSS Laboratory Contrd Sample - SoG PBW Prep Blank -Water <br />LCSSD Laboratory Control Sample -Soil Duplkate PQV Practice) l]uangfagon Verification standartl <br />LCSW laboratory fidltld Sample -Water SOL Serial DfiuBOn <br />Blanks Verifies that tlrere -s ra w minimal canfambation in the prep memad w cefibration procedure. <br />Contrd Samples Verifies the acwracy of the meRgd. inducting iha prep procedure. <br />Duplicates Vedfias the predsion of the ktstrument anNOr matted. <br />SpkeslFOrtified Matrix Determines sample mabix intedererlces, R any. <br />Standard Verifies the vafidty of the calibration. <br />• w . <br />B Analyle cwceniradan detected et a value between MDL entl PDL. <br />H Analysis exceeded method hdd tlma. pH k e fieM test with an Immediate hold tlma. <br />R Pow spike recovery aceepted because the other spike In the set tell wiNin the given limits. <br />T High Relafive Percent DiRerence (RPD) accepted because sample cencentratlons are less than tOx the MDL. <br />U Analyse was analyzed for but rib detected at the Mzficated MDL <br />V High blank data ecceptetl because sample Wncenbatlon is 10 times higher than blank cencenVatlon <br />W Pow recovery for SINer quafiy cenOrol is accepted because Sliver often predpitales with Chloride. <br />X Quality control sample W out of control. <br />Poor spike recovery is accepted because sample concentration M tar times greatw gran spike concentration. <br />(1) EPA 600/4A3-020. Methods for Chemical Analysisct Water arM Wastes, March 1963. <br />(2) EPA 600/8-93-100. Methods for the Determination of Inorganic Substances in EnvironmenW Samples, August 1993. <br />(3) EPA60018-9A-111. Methods for the Delerminatzm oT Metak in C-mnonmeMal Samples - Supplemem I, May 1994. <br />(5) EPA SW-046. Test Methods for Evaluating Solid Waste, ThiM EtliGon with Update III, December 1996. <br />(6) Standard Methods for the Examinatlon of Water and Wastewater, 19th edigon, 1995. <br />(1) DC results celwlaletl from raw Oata. Results may vary slightly if the rountletl values are used in me ralwlations. <br />(2) Soil, Sludge, and Plant matrices for Inorganic anayses ere reported on a dry weight basis, <br />(3) Animal matrices for Inorganic analyses are reported on an'as received" basis. <br />REPIN03.11.00.01 <br />L58465: Page 17 of28 <br />