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§ 136.3 40 CFR Ch. 1 (7-1-89 Edition) TABLE Il-REQUIRED CONTAINERS, PRESERVATYON TECHNIDUES, AND HOLDING TIMES-COn11nU0d - - ~ Parsrrala sb mama LOnbmd' Pmservelron • • Me.imum Mldng u'rn' a] Orgerc carbon .......... ....... .... .... .. P, G... Cool. PC, HCl d M,SOr to Do. pH <1. R P F•Ilrv Immed'elaly, GOd. ~ C. aB aorta .. {}nnylbannela .. .. .......... . . G Ronal and Norse roaare0 ......................... Analyse Immo d e y. to Orygan, Dafolved Prone........_..........._.... lop tb ............. Frs w use era side rn dart.... 5 hwn e] WIntM ...... ................... ........................ . G Doty............ Cod, a'C. Hr`''O, to PH c2 ... 20 days .! PnaMb .......... ..... ....... .. ........... ..... .. G .. ... Cod. e'L .. ................. . ee Mraf. a9 pnosoromf lelementsll ............... ......... ................ . P G Lod, a'C, H,SO, to PNC2 .... ]B data. 50 PM+phduf. Ialal . ......... ..... .......... .. ............ .. , P G Lod. e'C ... ..... .... .............. ] UeYe ....... ...... ................... .. ..... 5] Refrct+a. total. ..... ..... . P G .. .. do..... .............................. eta Sa Refid+. F,Ilereda ..................................... .............. . P G ......do................................. .. / daYf 55 Raactfe. Nmlreaada lTSSI ........ .. ...... ........ ............. . ....... .............. do aB own Se Reaaue. Seeleebla ............. ....................... P. G............ ................. ..... . .. ... do ] tlayf 5]. Reasba. Matta .................................... ..... . G............... . ........_............... ....... .. ......do......... ... ............................ 29 QYYa. 61. SACa ............................ ...... ..... .. ................. ...... .......... . G ... do..... ..... ............. ........ ... Do. BI Spenilrc tdNrcbnw... _ ............................. .._.......... . P G ................... ...... . do Do. eS Srltlale ... .................... ............ .. ................. ........... . . P G ........... . ..... Cod. e'L e0d irnc epelele ]data. EB SdIM .......... ....................... ..... .... .. .... ............. , plus epdmm hyctodde ID ............ P G pH> e. Non. repurrad ..... AneMe immediately. ..................................... ..... e] swlrle ............... . .. ............. P G Cad. a'C. .... ............................ ae nw.. .................. .. !A. SuHOClan1/ ....... ..... ................... .. . . .......... P G Ndu raVU..d ............................. AneMs ee Tar'peraN........._ ..............................._......... ... . . . .. ... P D .......... Lad. e'C............... ...... ... ee nod.. ]0 Tuhany .............._.............................. ............... . .. . ... . Taal IL-QrgarC TMf.• Y6-2o. 21. 2a-ge. ]a-]T, 39-e], eSiT, 1] G. Totten- Cad. A'G, O Wax Nb.SA..•.... 14 deYS. , 56. 88. Be, Be. YS-ei. Dl PdYJeade Msb Ilrod septum urbom. e, 57, 90. gagsads aramaYC Mctocarbone ..............ea............. ]. e, Acrdwrr era ecrydornuJe ............ .... .. ....... ro............. 2]. 00, aa. AB, 50, e], ]0, ]1. B0, e5, BB G, Telbm Pnerralf , r Yned cep. ]. ]5 BMardref" .. .. .... ...... .. .................... .. .. do .. .. ...... Ie, 11. eB, SrY51 FTVUIeIa salsa" ..... .. ........ ......d0......... .... ]2-)Y NrbOfelTwwrvr• ..... ...... .......... ............ do.......... ]B-e1. PCBs" adYbabda ..... ....... ................. ..... do ..... M. S5, 65. BB NrlrWrdtuYCe era uoptldona"...... do......... 1, 2 5, a-12, ]2, 00. Se, Se, 6a. 6B, 81, BB ......po... Py/IArcba vomalic IryJrouNmf ". 15. 1d 21, Ol, )5 Hebslnaf " ......................... ......do.. za. ]s-]T, eo-M, ol. Lhldiralea Yryaoca- ..... aD. bonf' •. do e] T13]D'• .......................... .. ............ ................. .. ...... Tape ID-Peetkaea Loa: I -]0 Peayrdea " . ..................................... ..... do.. LW IE-Rad'nbpLal Tob: 1-e AIpN, beta era rectum .... .............. ........... .. P. G... God. a'C, 0008% Ne.Srgc, Do. Hcl 10 pN2• Cod. a'C. OODBx Ns.Sr0.•. Do Adluft pH lD ~-5'°. Cod, a-G. OOOe% Nsr5,0.•.... rscddt ] l y alt r tlaya a0 eshaclian. ... ..tla .... ... ................ ...... ..... ] tleys oasts eabeclbnu Cod, A'C ...... ..................._..... 7 ante unW efbacSoA t0 days slier a.vedlon. a'C aloe m dot 00 Cool, 0000% Ner5r0.•. cod..•c_ ................. ........ oD Cool, a•C. ODOBx Ne,Sr0.' Do. afore 'n dent. ..... do .. ... .. ................_...... ..... Do. .. .. Cod. e'c, O.OOex Ne.$r0.•..... Do. ..... .. ...... .. Cod. A'G .............. .. ............... . Do. ....... .. .. riOd, a'C. 0000% NuSr0.'... Da. ..... . Cad. a'C. pN 5-e " ..... ....... .. Do .. ... HNQ 1a Pllcz ......... ... ....... . a monlna . __ T.er.u NaW 'POryeOrylerr IPI d Gbo IGI H Immedulah upon aampb cdleclan For cemlaosrle cnemcsl mmplse sear 'Samya preeanelbn aM'Atl G pe amwd po eYgsbl error a peaaved al Ura 9rrre d colleCWrl Wllan um mbirJn dst~IC unirlplrnmpouUnYlend samples aPror'0 6 elan atduol, pan cMnaca aempln msY M Peaened by g c o-IM .ally„ ant urrWa la to ba snipped by m^'^'^^ da"'a d fens ilrwggn Ilra Urvtbd Slalea Mails, rl moat compty w+ nenanmerd of Tranaponarw Harerddn Mauneb Regdetione Ise CFR Pen 1]1) Tne paaon ollennn0g auto maledY b bareponabon la refpduMa Id aneurNq auuT Gomplynca. For ine Peaervellw retanrorMnb of Tade I1. Iha OOka d Hvardda Mstaah. Ma,aeb Traefpolaibn Breeeu. DpenmWenl of Tgnspolebon nee dalamned Inat Ina He[adae Maa10N ReQteeuda do rola~ L~ gre^a s aj 11 slnG add (IINO,1 bw a of dulnna el concenlba onffol O ISX M oldf OOax by ream d bff (pH m rnlM wblbm al CIXCenbelbns of 005% b/ weans d efe d bff IPH about 1 d7 d eelal: Sulfuric acid IM.SO.1 e a bff ahM 1.15 a Ynslw% and Soa°^ bN'o'aa (NeOH) it vetm foNlw^s s1 cdreenbflims of O.OBO% tri W qnl ebdA 11 ]0 d el~ 'Semple flvaAd bs aneryt~ act ~ O~~W vaWd. Sarnpbf may Ds netlyto beer nperoda wh II Ina lparmiYtln, b mry b hold betas arery'ea 280 Environmental Prolecfion Agency § 136.4 morvlnnrq Inberalory, nes dale on Isle to show Ines iha epec,lrc rypea of samples uMa study ere stable Id ma blger time, era t4a roceNad a redence hem Ina Regronel Admmiabatd user f 1]e.]Ia) Soma famplea may not bD aehla Id Ina mormum Irmb perlotl eivnn In Ilre testa A pamrllee, or mbnildlrq lebdeldy, b WIIge1M 10 MM the Temple la a aMnor yme II tmWletlYe enfls to snow snot INa is necessaryry to mainleln ample iletgllry. SoD l 1]6 ](e) ld tlalab ' SndUtl only be used In Ina pnseucD nI msuldU chbrrrre •Manmum Mltlirg lima b 1e noon wnen sullidn Is prmanl. Oplmnall~ ell samploa may he tested won load ncdala pepm pelda pM edpNimnnb in dtlor to delarminn II sullao is pnfonl. II eul Ne a present, II can be removra W Ina edYynn of gdm.lm rubele powder uulll a nupauvn spot lost Is oblelnad. lIN eample n IJIaW aN loon NaOM Is 0odetl to psi 12 'samploa slauld ba IdlerM Immdynbtly nRSdn bosom etln~ngg ppmnrvelrve Id dnsolnd motels 'Guidmrcn nlyrum In mmploa In hn nnpnrd LY GC, LC, or GLYMS Id ap'•olm compounds. 'Sample mcorving no pll nUl"sln~nnl muvl M ennlpmtl wlllen seven tleya d eenaling '•Thn d1 ntljrntmonl n not lepu'rml d andom will not be meeaadtl Senalea Id 9up191n receirmg no pit edryslmonl must be enelytad wlllnn ] daYf nl samplnlg9. ' When the etlredeble analyses of concom tall wrlh,n a ingla cnemcsl category, ine spenlletl ~mservelrve eM maamum Mbing Iunua fM,ra ba nbxned td oplnnum asl¢guanl 01 sample Inlepriry Wnen Ina anarytes o roncam tall Wilnin Iwo or mde cnammal rAleporros, lire sample may be preserved by coolnq ID a'C, rndudnA residual chla,rlno wUn 0.000% sodium IM1OSUIIeIe, slwng m the tlor F, ems etllusling the pH l0 6-9: famplea geserved in Ibs manner may ne hDIJ Id (even days balers eMractinn antl for Idly ddye alter evlmdion Euepliom to Ibs opbonnl prosdvalion end nolAng limo procedwe ere nolM m Ioo1n01e 5 pe Ina lequirement fur Nloaullale /edKllon OI refau6l cnldmal, end loDlnplD9 12. IJ Ire l e anarysn of bemiUma/. '•II 1,1~ctphenylhydrenne b YFery ID ne present edlufl Ina pH al ln0 anrtrph to x0302 lg p0venl resnengemanl to 11a ,SpInB EWects may he flded up to ] tleyf balde anBlYaia d aldage b contluded user an Inen IO.idanl-yeG) elmmpnare "For Iha arulyua OI diplrenylnllroaemrrra. add S.OOB% Ne.arQ anU atljusl pM la 7-10 vnth NaOM wilMn to nods of MmpYrp 7The pH adluslmonl may be perldmetl upon racerpl st ine laboratoryry antl met be ortulled U Ina 9emplea ere efbacled plnln ]2 Mdf of collodion Fd Ina enplym of 91da, Wd U OOB% N05.Or. • 130 FR 2@760, OcL. ]G, IB73, as amenAeA at 41 FR 52781, Dec, 1, IB76: 9B FR 93251, 43258, 93259, Oct. 26, l@89; 50 FR 691, 692, 895, Jnn. 4, 1905; 61 FR 23G93, June 30, 1808; 52 FR 33593, Sept. 3, IBB71 EmrontAl. NDTB: Information collection requfremenls cons nlned In 4 136.3fe) have not been approved by Llle Office of Management and Budget antl are not effective, pending OMB approval. O 136.4 Appliculion fur nllernole leaf pro- ecduree. (a) Any person may apply Lo Lhe Re- gional AdminlsLrntor lu the Region where the discharge occurs fur approv- al of an alternative Lest procedure. (b) When Lhe discharge for which an allernaLive test procedure Is proposed occurs wlLhin a Slate having a permit pr gram approved pursuant Lo section 402 of Lhe Act, Lhe applicant shall su}Imit his appllcatlon to the Regional A ''nlnlstrator through the Director of ll ~ State agency having responslbllity for Issuance of NPDES permits wlthln xUCh $taLe. (c) Unless and until printed appllca- tlon forms are made avallxble, an ap- pllcatlon for nn alternate Lest proce- dure may be made by IeLter In Lrlpll- cate. Any appllcatlon for an alternate test Pr(1CCQUYE ilnaer Lhis paragraph ICI 911x11: (1) Provide the name and address of the responsible person or flan making the discharge ll[ not Lhe applicanU alld the npplicablc ID number of the exlsLing or pending penal L, Issuing agency, and type of permlL for whlclt the alternate Lest procedure Is request- ed, and the discharge scrlal number. (2) Identify the pollutant pr parame- ter for which approvai o[ an nlLernate testing procedure is being requested. (3) Provide JustlflcnLlon for using testing procedures other Lhan those specltled In Table I. (9) Provide a detailed descrlpLlon of the proposed alternate Lest procedure, together with references Lo published studies of Lhe applicability of Lhe al- ternate test procedure Lo Lhe e[fluenls In qucstlon. (d) An appllcatlon for approval of an alternate Lest procedure for natlon- wlde use may be made by IeLter In trlp- Ilcate Lo the Director, Environmental Monitoring and Support Lnboralory, Clncinnatl, Ohio 45208. Any apPlica- tlon [or an alternate lest procedure under this paragraph (d) shall: (1) Provide the name end address o[ the responsible person or firm TQaking .the eppircatTon. (2) IdenLlfy the pollutnnL(s) Or parameter(s) for which nationwide ap- proval o[ an alternate testing proce- dure is bc{nH requested. (3) Provide a dclalled descrlPllon of the proposed alternate procedure, to- gether wIL11 references to published or other studies conflrnting Lhe general applicability of the nlterunte Lest pro- cedure Lo Lhe polluLanUs) or 281 •