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ACZ Laboratories, Inc. <br />2773 Downhill Drive Steamboat Springs, CO 80487 (800J 334-5493 <br />Twentymile Coal Co. ACZ Project ID: L59228 <br />L59228-01 WG214268 Sodium, dissolved <br />WG214343 Biwmonate as Bicarbonate <br />Carbonate as Carbonate <br />Hydroxide as Hydroxide <br />WG214239 Nitrale/Nitrite as N <br />WG214343 PH <br />pH measured at <br />WG214241 Phosphorus, ortho dissolvetl <br />WG214379 Resitlue. Fiteable (TOS) @180C <br />M200.71CP <br />SM23208 -Titration <br />SM2320B -Titration <br />SM2320B -Titration <br />SM2320B -Titration <br />SM2320B -Titration <br />SM2320B - Titmtion <br />M353.2 - H2SO4 preserved <br />M750.1 - Elec[rometdc <br />M150.1 - EleMrometdc <br />M150.7 - Electrometdc <br />M365.1 -Automated Ascorbic <br />Acid <br />M365.1 - Amomated Ascorbic <br />Acid <br />M3 The accuracy of the spike recovery does not apply because <br />anatyte concentration in the sample is disproportionate to <br />Ne spike level. The recovery of the method control sample <br />was acceptable. <br />Fi3 Sample was received and anayzed past holding time. <br />N7 See Case Nartaave. <br />H3 Sample was received and analyzed past holding time. <br />N1 Sea Case Nanative. <br />H3 Sample was received and anayzed past holding time. <br />N1 Sea Case Nanatrve. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is too low for <br />accurate evaluation (< 10x MDL). <br />N1 See Case Nanadve. <br />H3 Sample was received and analyzed past holding time. <br />N1 See Casa Narrative. <br />H3 Sample was received and anayzed past holding time. <br />RA Relative Percent Difference (RPD) was not used for data <br />validation because the sample concentration is loo low for <br />accurate evaluaton (< 10x MDL). <br />H3 Sample was received and anayzed past holding time. <br />ZO TDS concentaaon is based on a foal residua greater than <br />200 mg. <br />FD Sample was received and analyzed past holding time. <br />RA Relative Pement Difference (RPD) was not used for data <br />validation because the sample concentration is too knv /or <br />accurate evaluation (< 10x MDL). <br />RA Relative Percent Difference (RPD) was not usetl for data <br />validation because the sample concentration is loo low for <br />accurate evaluation (< 10x MDL). <br />H3 Sample was received and analyzed past holding time. <br />N1 See Case Narrative. <br />M760.1 - GmvimeMc <br />M760.1 - GrevimeMc <br />WG214387 Residue, Non-Filterable (TSS) @105C M160.2 - Grevimetdc <br />M160.2 - Gmvimetdc <br />WG214412 Sulfate SM4500 S04-0 <br />WG214343 Total Alkalinity SM2320B - Titration <br />SM2320B - Titratbn <br />REPAD.15.06.06.01 <br />L59228: Page 6 of 8 <br />